3-(4-chlorophenyl)-N′-(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)-4,6-dimethoxy-1H-indole-7-carbohydrazide

Base Information

• Chemical Name: 3-(4-chlorophenyl)-N′-(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)-4,6-dimethoxy-1H-indole-7-carbohydrazide
• CAS No.: 1445801-61-5
• Molecular Formula: C₃₄H₂₈Cl₂N₄O₆
• Molecular Weight: 659.526

Synonyms:3-(4-chlorophenyl)-N′-(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)-4,6-dimethoxy-1H-indole-7-carbohydrazide

Chemical Property of 3-(4-chlorophenyl)-N′-(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)-4,6-dimethoxy-1H-indole-7-carbohydrazide

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Technology Process of 3-(4-chlorophenyl)-N′-(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)-4,6-dimethoxy-1H-indole-7-carbohydrazide

There total 3 articles about 3-(4-chlorophenyl)-N′-(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)-4,6-dimethoxy-1H-indole-7-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

3-(4-chlorophenyl)-4,6-dimethoxy-7-trichloroacetyl-1H-indole → 3-(4-chlorophenyl)-N′-(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)-4,6-dimethoxy-1H-indole-7-carbohydrazide (1445801-61-5)

Guidance literature:

With hydrazine hydrate; triethylamine; In acetonitrile; for 24h; Reflux;

DOI:10.1016/j.bmc.2014.01.025

Reference yield:

3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole (151290-21-0) → 3-(4-chlorophenyl)-N′-(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)-4,6-dimethoxy-1H-indole-7-carbohydrazide (1445801-61-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 1,2-dichloro-ethane / 3 h / Reflux

2: hydrazine hydrate; triethylamine / acetonitrile / 24 h / Reflux

With hydrazine hydrate; triethylamine; In 1,2-dichloro-ethane; acetonitrile;

DOI:10.1016/j.bmc.2014.01.025

Reference yield:

3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbohydrazide (1569642-73-4) + 3-(4-chlorophenyl)-4,6-dimethoxy-7-trichloroacetyl-1H-indole → 3-(4-chlorophenyl)-N′-(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)-4,6-dimethoxy-1H-indole-7-carbohydrazide (1445801-61-5)

Guidance literature:

With triethylamine; In acetonitrile;

DOI:10.1039/c4ob00460d

upstream raw materials:

3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole

3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbohydrazide

Downstream raw materials:

2,5-di(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indol-7-yl)-1,3,4-oxadiazole

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