POC₆H₂-2,4,6-t-Bu₃

Base Information

Chemical Name:POC₆H₂-2,4,6-t-Bu₃
CAS No.:796-62-3
Molecular Formula:C₁₈H₂₉Cl₂OP
Molecular Weight:363.307
Hs Code.:

POC<sub>6</sub>H<sub>2</sub>-2,4,6-t-Bu<sub>3</sub>

Synonyms:POC₆H₂-2,4,6-t-Bu₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of POC₆H₂-2,4,6-t-Bu₃

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Technology Process of POC₆H₂-2,4,6-t-Bu₃

There total 1 articles about POC₆H₂-2,4,6-t-Bu₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 732-26-3
2,4,6-tri-tert-butylphenoxol

: 796-62-3
POC₆H₂-2,4,6-t-Bu₃

Guidance literature:: With triethylamine; phosphorus trichloride; In toluene; at 25 ℃; for 24h;
DOI:10.1016/0022-328X(90)80007-M

Reference yield: 100.0%

: 796-62-3
POC₆H₂-2,4,6-t-Bu₃

: C₁₈H₃₁OP*BH₃

Guidance literature:: With lithium borohydride; In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.1039/b202361j

Reference yield: 100.0%

: lithium borohydride

: 796-62-3
POC₆H₂-2,4,6-t-Bu₃

: 475636-41-0
[(2,4,6-t-Bu₃C₆H₂O)PH₂]BH₃

Guidance literature:: In tetrahydrofuran; under N2; a soln. of (((CH3)3C)3C6H2O)PCl2 in C4H8O was added dropwise to a suspn. of Li(BH4) in C4H8O at 0°C; the mixt. was warmed to 25°C and stirred for 16 h; the volatiles was removed in vac., the residue was extd. with hexanes and filtered through Celite, the solvent was removed, the residue was dried in vac.;
DOI:10.1039/b202361j