N,N-Bis(2-hydroxyethyl)-p-phenylenediamine sulphate

Base Information

• Chemical Name: N,N-Bis(2-hydroxyethyl)-p-phenylenediamine sulphate
• CAS No.: 54381-16-7
• Molecular Formula: C10H16N2O2^.H2SO4
• Molecular Weight: 294.329
• Hs Code.: 29309090
• European Community (EC) Number: 259-134-5
• UNII: 3X5A8DP6HC
• DSSTox Substance ID: DTXSID5020075
• Wikidata: Q27258167
• RXCUI: 1427230
• Mol file: 54381-16-7.mol

Synonyms:54381-16-7;2,2'-((4-Aminophenyl)azanediyl)diethanol sulfate;N,N-Bis(2-hydroxyethyl)-p-phenylenediamine sulphate;N,N-Bis(2-hydroxyethyl)-1,4-phenylenediamine sulfate;N,N-Bis(2-hydroxyethyl)-p-phenylenediamine sulfate;CCRIS 7702;Ro 371;2-[4-amino-N-(2-hydroxyethyl)anilino]ethanol;sulfuric acid;EINECS 259-134-5;2,2'-[(4-Aminophenyl)imino]bisethanol sulfate;UNII-3X5A8DP6HC;3X5A8DP6HC;(p-Ammoniophenyl)bis(2-hydroxyethyl)ammonium sulphate;T 32;4-Amino-N,N-di(beta-hydroxyethyl)aniline sulfate;Ethanol, 2,2'-((4-aminophenyl)imino)bis-, sulfate (1:1) (salt);2,2'-((4-Aminophenyl)imino)bis(ethanol) sulfate;MFCD00013177;N,N-Bis-(2-hydroxyethyl)-p-phenylenediamine sulfate;2,2'-((4-Aminophenyl)imino)bisethanol sulfate (salt);N,N-Bis(beta-hydroxyethyl)-p-phenylenediamine sulfate;N,N-Bis-2-hydroxyethyl-p-fenylendiamin siran [Czech];63886-75-9;2-(N-p-Aminophenyl-N-2-hydroxyethylamino)ethanol sulfate;Ethanol, 2,2'-((4-aminophenyl)imino)bis-, sulfate (salt);p-Phenylenediamine, N,N-bis(2-hydroxyethyl)-, sulfate (1:1);Ethanol, 2,2'-[(4-aminophenyl)imino]bis-, sulfate (1:1) (salt);N,N-Bis-2-hydroxyethyl-p-fenylendiamin siran;2,2'-((4-Aminophenyl)imino)bisethanol sulfate;2,2'-[(4-aminophenyl)imino]diethanol sulfate (salt);C10-H16-N2-O2.H2-O4-S;COLOREX NNBIS;JAROCOL BHP;2,2'-((4-Aminophenyl)azanediyl)diethanolsulfate;2,2-[(4-Aminophenyl)azanediyl]diethanol sulfate;SCHEMBL624610;DTXSID5020075;C10H16N2O2.H2O4S;RO-371;AKOS015889668;CS-W019182;CS-17386;LS-66439;LS-66440;N,N-Bis(2-hydroxyethyl)-p-phenylenediami;SY112843;LS-105836;FT-0629415;2,2'-(4-aminophenylazanediyl)diethanol sulfate;N,N-Bis(2-hydroxyethyl)-4-phenylenediamine sulfate;N,N-Di-(2-hydroxyethyl)-p-phenylenediamine sulfate;W-105633;Q27258167;N,N'-Bis(2-hydroxyethyl)-p-phenyl-ene-diamine sulphate;ETHANOL, 2,2'-((4-AMINOPHENYL)IMINO)BIS-, SULFATE;N1, N1-BIS(HYDROXYETHYL)-P-PHENYLENEDIAMINE SULFATE;ETHANOL, 2,2'-((4-AMINOPHENYL)IMINO)BIS-, SULPHATE;N,N-BIS(BETA-HYDROXY ETHYL)-P-PHENYLENEDIAMINE SULFATE;N1, N1-BIS(HYDROXYETHYL)-P-PHENYLENEDIAMINE SULPHATE;2-[(4-aminophenyl)(2-hydroxyethyl)amino]ethan-1-ol;ETHANOL, 2,2'-((4-AMINOPHENYL)IMINO)BIS-, SULPHATE (SALT);Ethanol, 2,2'-(1,4-phenylenediimino)bis-, sulfate (1:1) (salt);N,N-bis(2-hydroxyethyl)-1,4-phenylenediamine sulfate, AldrichCPR;N,N-BIS(2-HYDROXYETHYL)-P-PHENYLENEDIAMINE SULFATE [INCI];ETHANOL, 2,2'-((4-AMINOPHENYL)IMINO)BIS-, SULPHATE (1:1) (SALT)

Chemical Property of N,N-Bis(2-hydroxyethyl)-p-phenylenediamine sulphate

Chemical Property:

• Appearance/Colour: White crystal powder
• Vapor Pressure: 65Pa at 20℃
• Melting Point: 168-171°C
• Boiling Point: 416.4 °C at 760 mmHg
• Flash Point: 205.6 °C
• PSA: 152.70000
• Density: 1.497[at 20℃]
• LogP: 1.06900
• Storage Temp.: Keep in dark place,Sealed in dry,Room Temperature
• Solubility.: Acetonitrile (Slightly), DMSO (Slightly)
• Water Solubility.: 178g/L at 20℃
• Hydrogen Bond Donor Count: 5
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 5
• Exact Mass: 294.08855747
• Heavy Atom Count: 19
• Complexity: 222

Purity/Quality:

99% ^*data from raw suppliers

2,2''-((4-Aminophenyl)azanediyl)diethanolSulfate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): T
• Hazard Codes: T
• Statements: 25
• Safety Statements: 45

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1N)N(CCO)CCO.OS(=O)(=O)O
• Uses: 2,2''-((4-Aminophenyl)azanediyl)diethanol Sulfate is a useful compound in hair dye. Has cosmetic applications.

Technology Process of N,N-Bis(2-hydroxyethyl)-p-phenylenediamine sulphate

There total 1 articles about N,N-Bis(2-hydroxyethyl)-p-phenylenediamine sulphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ N,N-bis(2-hydroxyethyl)-1,4-phenylenediamine sulfate (54381-16-7)

Guidance literature:

Reference yield: 84.0%

N,N-bis(2-hydroxyethyl)-1,4-phenylenediamine sulfate (54381-16-7) → C20H28N4O4

Guidance literature:

With CotA laccase; In aq. phosphate buffer; ethanol; at 37 ℃; for 2h; pH=6; Green chemistry; Enzymatic reaction;

DOI:10.1002/asia.201801450

Reference yield:

2-[3-(5-chloro-2,4-dinitrophenylamino)pyrazolo[1,5-a]pyridin-2-yloxy]ethanol + N,N-bis(2-hydroxyethyl)-1,4-phenylenediamine sulfate (54381-16-7) → 2-[3-(5-{4-[bis(2-hydroxyethyl)amino]phenylamino}-2,4-dinitrophenylamino)pyrazolo[1,5-a]pyridin-2-yloxy]ethanol

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In 1-methyl-pyrrolidin-2-one; at 100 ℃; for 2h; Inert atmosphere;

Refernces

• 1、 -. "Transition metal complexes as dye forming catalysts in hair coloring compositions". . . Retrieved 2008/06/13.
• 2、 -. "Nitrated coupler compounds useful in direct dyeing and simultaneous oxidation and direct dyeing of keratinic fibers". . . Retrieved 2008/06/13.