p-methylphenyl 2-deoxy-2-phthalimido-6-deoxy-6-azido-3,4-dibenzoyl-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:p-methylphenyl 2-deoxy-2-phthalimido-6-deoxy-6-azido-3,4-dibenzoyl-1-thio-β-D-glucopyranoside
CAS No.:817195-44-1
Molecular Formula:C₃₅H₂₈N₄O₇S
Molecular Weight:648.696
Hs Code.:

Synonyms:p-methylphenyl 2-deoxy-2-phthalimido-6-deoxy-6-azido-3,4-dibenzoyl-1-thio-β-D-glucopyranoside

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Chemical Property of p-methylphenyl 2-deoxy-2-phthalimido-6-deoxy-6-azido-3,4-dibenzoyl-1-thio-β-D-glucopyranoside

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Technology Process of p-methylphenyl 2-deoxy-2-phthalimido-6-deoxy-6-azido-3,4-dibenzoyl-1-thio-β-D-glucopyranoside

There total 6 articles about p-methylphenyl 2-deoxy-2-phthalimido-6-deoxy-6-azido-3,4-dibenzoyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 817195-38-3
C₃₅H₂₉NO₈S

: 817195-44-1
p-methylphenyl 2-deoxy-2-phthalimido-6-deoxy-6-azido-3,4-dibenzoyl-1-thio-β-D-glucopyranoside

Guidance literature:: C₃₅H₂₉NO₈S; With pyridine; p-toluenesulfonyl chloride; at 50 ℃; for 0.416667h;

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium azide; In DMF (N,N-dimethyl-formamide); at 50 ℃; for 3h;

Reference yield: 1.45%

: C₄₂H₃₅NO₁₀S₂

: 817195-44-1
p-methylphenyl 2-deoxy-2-phthalimido-6-deoxy-6-azido-3,4-dibenzoyl-1-thio-β-D-glucopyranoside

Guidance literature:: With sodium azide; In N,N,N,N,N,N-hexamethylphosphoric triamide; N,N-dimethyl-formamide; at 50 ℃; for 3h;
DOI:10.1002/anie.200462003

Reference yield:

: 2-[(2S,3R,4R,5S,6R)-6-(tert-Butyl-diphenyl-silanyloxymethyl)-4,5-dihydroxy-2-p-tolylsulfanyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

: 817195-44-1
p-methylphenyl 2-deoxy-2-phthalimido-6-deoxy-6-azido-3,4-dibenzoyl-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 4 h

2: 2.52 g / HF/pyridine / 0.08 h

3: pyridine / 0.25 h

4: 1.45 percent / NaN₃ / dimethylformamide; hexamethylphosphoric acid triamide / 3 h / 50 °C

With pyridine; sodium azide; hydrogen fluoride; In N,N,N,N,N,N-hexamethylphosphoric triamide; N,N-dimethyl-formamide;
DOI:10.1002/anie.200462003