4-{4-[(tert-butoxycarbonyl)methoxycarbonyl]phenyl}-4-azatricyclo[5.2.1.0^2,6]dec-8-ene

Base Information

• Chemical Name: 4-{4-[(tert-butoxycarbonyl)methoxycarbonyl]phenyl}-4-azatricyclo[5.2.1.0^2,6]dec-8-ene
• CAS No.: 1173823-47-6
• Molecular Formula: C₂₂H₂₇NO₄
• Molecular Weight: 369.461

Synonyms:4-{4-[(tert-butoxycarbonyl)methoxycarbonyl]phenyl}-4-azatricyclo[5.2.1.0^2,6]dec-8-ene

Chemical Property of 4-{4-[(tert-butoxycarbonyl)methoxycarbonyl]phenyl}-4-azatricyclo[5.2.1.0^2,6]dec-8-ene

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Technology Process of 4-{4-[(tert-butoxycarbonyl)methoxycarbonyl]phenyl}-4-azatricyclo[5.2.1.0^2,6]dec-8-ene

There total 1 articles about 4-{4-[(tert-butoxycarbonyl)methoxycarbonyl]phenyl}-4-azatricyclo[5.2.1.0^2,6]dec-8-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-(4-aza-tricyclo[5.2.1.02,6]dec-8-en-4-yl)benzoic acid (877154-50-2) + bromoacetic acid tert-butyl ester (5292-43-3) → 4-{4-[(tert-butoxycarbonyl)methoxycarbonyl]phenyl}-4-azatricyclo[5.2.1.02,6]dec-8-ene (1173823-47-6)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 0.5h;

DOI:10.1002/chem.200900195

Reference yield: 91.0%

4-{4-[(tert-butoxycarbonyl)methoxycarbonyl]phenyl}-4-azatricyclo[5.2.1.02,6]dec-8-ene (1173823-47-6) → 4-{4-[(hydroxycarbonyl)methoxycarbonyl]phenyl}-4-azatricyclo[5.2.1.02,6]dec-8-ene (1173823-48-7)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 3h;

DOI:10.1002/chem.200900195

upstream raw materials:

4-(4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yl)benzoic acid

bromoacetic acid tert-butyl ester

Downstream raw materials:

4-{4-[(hydroxycarbonyl)methoxycarbonyl]phenyl}-4-azatricyclo[5.2.1.0^2,6]dec-8-ene

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