Phthalic acid 1-((2S,3R,4S)-5-tert-butoxycarbonylamino-2,3,4-trimethoxy-pentyl) ester 2-pentachlorophenyl ester

Base Information

Chemical Name:Phthalic acid 1-((2S,3R,4S)-5-tert-butoxycarbonylamino-2,3,4-trimethoxy-pentyl) ester 2-pentachlorophenyl ester
CAS No.:194663-63-3
Molecular Formula:C₂₇H₃₀Cl₅NO₉
Molecular Weight:689.802
Hs Code.:

Synonyms:Phthalic acid 1-((2S,3R,4S)-5-tert-butoxycarbonylamino-2,3,4-trimethoxy-pentyl) ester 2-pentachlorophenyl ester

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Chemical Property of Phthalic acid 1-((2S,3R,4S)-5-tert-butoxycarbonylamino-2,3,4-trimethoxy-pentyl) ester 2-pentachlorophenyl ester

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Technology Process of Phthalic acid 1-((2S,3R,4S)-5-tert-butoxycarbonylamino-2,3,4-trimethoxy-pentyl) ester 2-pentachlorophenyl ester

There total 3 articles about Phthalic acid 1-((2S,3R,4S)-5-tert-butoxycarbonylamino-2,3,4-trimethoxy-pentyl) ester 2-pentachlorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85-44-9
phthalic anhydride

: 194663-63-3
Phthalic acid 1-((2S,3R,4S)-5-tert-butoxycarbonylamino-2,3,4-trimethoxy-pentyl) ester 2-pentachlorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: DMAP / pyridine / 24 h / 40 °C

2: 8.8 g / dicyclohexylcarbodiimide / ethyl acetate / 72 h

With dmap; dicyclohexyl-carbodiimide; In pyridine; ethyl acetate;
DOI:10.1016/S0008-6215(97)00122-5

Reference yield:

: 1-(tert-butoxycarbonylamino)-1-deoxy-2,3,4-tri-O-methyl-L-arabinitol

: 194663-63-3
Phthalic acid 1-((2S,3R,4S)-5-tert-butoxycarbonylamino-2,3,4-trimethoxy-pentyl) ester 2-pentachlorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: DMAP / pyridine / 24 h / 40 °C

2: 8.8 g / dicyclohexylcarbodiimide / ethyl acetate / 72 h

With dmap; dicyclohexyl-carbodiimide; In pyridine; ethyl acetate;
DOI:10.1016/S0008-6215(97)00122-5