[4-(tert-butoxycarbonylamino-methyl)-2,5-bis-dodecyloxy-benzyl]-carbamic acid tert-butyl ester

Base Information

• Chemical Name: [4-(tert-butoxycarbonylamino-methyl)-2,5-bis-dodecyloxy-benzyl]-carbamic acid tert-butyl ester
• CAS No.: 861108-82-9
• Molecular Formula: C₄₂H₇₆N₂O₆
• Molecular Weight: 705.075

Synonyms:[4-(tert-butoxycarbonylamino-methyl)-2,5-bis-dodecyloxy-benzyl]-carbamic acid tert-butyl ester

Chemical Property of [4-(tert-butoxycarbonylamino-methyl)-2,5-bis-dodecyloxy-benzyl]-carbamic acid tert-butyl ester

Chemical Property:

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Technology Process of [4-(tert-butoxycarbonylamino-methyl)-2,5-bis-dodecyloxy-benzyl]-carbamic acid tert-butyl ester

There total 2 articles about [4-(tert-butoxycarbonylamino-methyl)-2,5-bis-dodecyloxy-benzyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-bis(dodecyloxy)-2,5-diiodobenzene (145483-66-5) → [4-(tert-butoxycarbonylamino-methyl)-2,5-bis-dodecyloxy-benzyl]-carbamic acid tert-butyl ester (861108-82-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 83 percent / HMPA / 3 h / Heating

2: LiAlH₄ / tetrahydrofuran / 12 h / Heating

3: 73 mg / CH₂Cl₂

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja0524088

Reference yield:

4-aminomethyl-2,5-bis-dodecyloxy-benzylamine (861108-84-1) + di-tert-butyl dicarbonate (24424-99-5) → [4-(tert-butoxycarbonylamino-methyl)-2,5-bis-dodecyloxy-benzyl]-carbamic acid tert-butyl ester (861108-82-9)

Guidance literature:

In dichloromethane;

DOI:10.1021/ja0524088

Reference yield:

[4-(tert-butoxycarbonylamino-methyl)-2,5-bis-dodecyloxy-benzyl]-carbamic acid tert-butyl ester (861108-82-9) + trifluoroacetic acid (76-05-1) → 4-aminomethyl-2,5-bis-dodecyloxy-benzylamine; compound with trifluoro-acetic acid

Guidance literature:

In dichloromethane; at 0 ℃; for 3h;

DOI:10.1021/ja0524088

upstream raw materials:

4-aminomethyl-2,5-bis-dodecyloxy-benzylamine

di-tert-butyl dicarbonate

1,4-bis(dodecyloxy)-2,5-diiodobenzene

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