butyl 2-(phenylthiocarbonyl)butanoate

Base Information

Chemical Name:butyl 2-(phenylthiocarbonyl)butanoate
CAS No.:1319740-98-1
Molecular Formula:C₁₅H₂₀O₃S
Molecular Weight:280.388
Hs Code.:

Synonyms:butyl 2-(phenylthiocarbonyl)butanoate

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Chemical Property of butyl 2-(phenylthiocarbonyl)butanoate

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Technology Process of butyl 2-(phenylthiocarbonyl)butanoate

There total 3 articles about butyl 2-(phenylthiocarbonyl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 16855-58-6
S,S'-diphenyl 2-ethyldithiomalonate

: 71-36-3
butan-1-ol

: 1319740-98-1
butyl 2-(phenylthiocarbonyl)butanoate

Guidance literature:: With C₈H₆O₄^(2-)*Cu⁽²⁺⁾; In acetonitrile; at 60 ℃; for 5h; Molecular sieve; air;
DOI:10.1021/ol201744u

Reference yield:

: 55552-69-7
2-ethylmalonyl dichloride

: 1319740-98-1
butyl 2-(phenylthiocarbonyl)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0.17 h / 0 - 20 °C / air

2: C₈H₆O₄^(2-)*Cu⁽²⁺⁾ / acetonitrile / 5 h / 60 °C / Molecular sieve; air

With C₈H₆O₄^(2-)*Cu⁽²⁺⁾; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/ol201744u

Reference yield:

: 601-75-2
ethylmalonic acid

: 1319740-98-1
butyl 2-(phenylthiocarbonyl)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 3 h / Reflux; air

2: triethylamine / dichloromethane / 0.17 h / 0 - 20 °C / air

3: C₈H₆O₄^(2-)*Cu⁽²⁺⁾ / acetonitrile / 5 h / 60 °C / Molecular sieve; air

With thionyl chloride; C₈H₆O₄^(2-)*Cu⁽²⁺⁾; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/ol201744u