(2R,5Z,8S,9R)-8-benzyloxy-9-hydroxymethyl-2-methoxy-2-vinyl-2,3,4,7,8,9-hexahydrooxonine

Base Information

Chemical Name:(2R,5Z,8S,9R)-8-benzyloxy-9-hydroxymethyl-2-methoxy-2-vinyl-2,3,4,7,8,9-hexahydrooxonine
CAS No.:1172121-93-5
Molecular Formula:C₁₉H₂₆O₄
Molecular Weight:318.413
Hs Code.:

Synonyms:(2R,5Z,8S,9R)-8-benzyloxy-9-hydroxymethyl-2-methoxy-2-vinyl-2,3,4,7,8,9-hexahydrooxonine

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Chemical Property of (2R,5Z,8S,9R)-8-benzyloxy-9-hydroxymethyl-2-methoxy-2-vinyl-2,3,4,7,8,9-hexahydrooxonine

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Technology Process of (2R,5Z,8S,9R)-8-benzyloxy-9-hydroxymethyl-2-methoxy-2-vinyl-2,3,4,7,8,9-hexahydrooxonine

There total 1 articles about (2R,5Z,8S,9R)-8-benzyloxy-9-hydroxymethyl-2-methoxy-2-vinyl-2,3,4,7,8,9-hexahydrooxonine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1172121-48-0
(2R,5Z,8S,9R)-8-benzyloxy-9-(tert-butyldiphenylsilanyloxymethyl)-2-methoxy-2-vinyl-2,3,4,7,8,9-hexahydrooxonine

: 1172121-93-5
(2R,5Z,8S,9R)-8-benzyloxy-9-hydroxymethyl-2-methoxy-2-vinyl-2,3,4,7,8,9-hexahydrooxonine

Guidance literature:: (2R,5Z,8S,9R)-8-benzyloxy-9-(tert-butyldiphenylsilanyloxymethyl)-2-methoxy-2-vinyl-2,3,4,7,8,9-hexahydrooxonine; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With water; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2009.03.010

Reference yield:

: 1172121-93-5
(2R,5Z,8S,9R)-8-benzyloxy-9-hydroxymethyl-2-methoxy-2-vinyl-2,3,4,7,8,9-hexahydrooxonine

: 1172121-94-6
(2R,5Z,8S,9R)-8-benzyloxy-2-methoxy-2-vinyl-2,3,4,7,8,9-hexahydrooxonine-9-carbaldehyde

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.03.010