(1R,2R,1'S,2''S)-2-[2-(2''-methoxymethylpyrrolidin-1-ylimino)-1'-methylethyl]-5-oxo-cyclopentanecarboxylic acid methylester

Base Information

Chemical Name:(1R,2R,1'S,2''S)-2-[2-(2''-methoxymethylpyrrolidin-1-ylimino)-1'-methylethyl]-5-oxo-cyclopentanecarboxylic acid methylester
CAS No.:205496-89-5
Molecular Formula:C₁₆H₂₆N₂O₄
Molecular Weight:310.393
Hs Code.:

Synonyms:(1R,2R,1'S,2''S)-2-[2-(2''-methoxymethylpyrrolidin-1-ylimino)-1'-methylethyl]-5-oxo-cyclopentanecarboxylic acid methylester

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Chemical Property of (1R,2R,1'S,2''S)-2-[2-(2''-methoxymethylpyrrolidin-1-ylimino)-1'-methylethyl]-5-oxo-cyclopentanecarboxylic acid methylester

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Technology Process of (1R,2R,1'S,2''S)-2-[2-(2''-methoxymethylpyrrolidin-1-ylimino)-1'-methylethyl]-5-oxo-cyclopentanecarboxylic acid methylester

There total 1 articles about (1R,2R,1'S,2''S)-2-[2-(2''-methoxymethylpyrrolidin-1-ylimino)-1'-methylethyl]-5-oxo-cyclopentanecarboxylic acid methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59983-39-0,187035-29-6
(S)-1-amino-2-(methoxymethyl)pyrrolidine

: 205496-89-5
(1R,2R,1'S,2''S)-2-[2-(2''-methoxymethylpyrrolidin-1-ylimino)-1'-methylethyl]-5-oxo-cyclopentanecarboxylic acid methylester

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) LDA; 2.) N,N,N',N'-tetramethylethylenediamine / 1.) THF, 0 deg C; 2.) THF, -78 deg C

With N,N,N,N,-tetramethylethylenediamine; lithium diisopropyl amide;
DOI:10.3987/COM-96-S2

Reference yield:

: 205496-89-5
(1R,2R,1'S,2''S)-2-[2-(2''-methoxymethylpyrrolidin-1-ylimino)-1'-methylethyl]-5-oxo-cyclopentanecarboxylic acid methylester

: 4581-74-2
neonepetalactone

Guidance literature:: Multi-step reaction with 4 steps

1: (C₂H₅)3N, DMPU

2: diethyl ether / -78 - 25 °C

3: aq. HCl / Ambient temperature

4: 65 percent / L-selectride / tetrahydrofuran / 1 h / -78 °C

With hydrogenchloride; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; L-Selectride; triethylamine; In tetrahydrofuran; diethyl ether;
DOI:10.3987/COM-96-S2