bis(4,4'-biphenylyl)ethynylmethanol

Base Information

Chemical Name:bis(4,4'-biphenylyl)ethynylmethanol
CAS No.:188429-39-2
Molecular Formula:C₂₇H₂₀O
Molecular Weight:360.455
Hs Code.:

Synonyms:bis(4,4'-biphenylyl)ethynylmethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(4,4'-biphenylyl)ethynylmethanol

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Technology Process of bis(4,4'-biphenylyl)ethynylmethanol

There total 2 articles about bis(4,4'-biphenylyl)ethynylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3478-90-8
4,4'-diphenylbenzophenone

: 1066-54-2
trimethylsilylacetylene

: 188429-39-2
bis(4,4'-biphenylyl)ethynylmethanol

Guidance literature:: trimethylsilylacetylene; With n-butyllithium; In tetrahydrofuran; at -78.16 ℃; for 0.25h;

4,4'-diphenylbenzophenone; In tetrahydrofuran; at -78.16 - 19.84 ℃; for 1.5h;

With potassium hydroxide; In methanol; at 20 ℃; for 1h; Further stages.;
DOI:10.1107/S010876810001154X