Octyl-O-(2,3,4-tri-O-acetyl-6-desoxy-α-D-mannopyranosyl)-(1->6)-2-O-benzyl-4-O-methyl-β-D-mannopyranosid

Base Information

• Chemical Name: Octyl-O-(2,3,4-tri-O-acetyl-6-desoxy-α-D-mannopyranosyl)-(1->6)-2-O-benzyl-4-O-methyl-β-D-mannopyranosid
• CAS No.: 146597-65-1
• Molecular Formula: C₃₄H₅₂O₁₃
• Molecular Weight: 668.779

Synonyms:Octyl-O-(2,3,4-tri-O-acetyl-6-desoxy-α-D-mannopyranosyl)-(1->6)-2-O-benzyl-4-O-methyl-β-D-mannopyranosid

Chemical Property of Octyl-O-(2,3,4-tri-O-acetyl-6-desoxy-α-D-mannopyranosyl)-(1->6)-2-O-benzyl-4-O-methyl-β-D-mannopyranosid

Chemical Property:

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Technology Process of Octyl-O-(2,3,4-tri-O-acetyl-6-desoxy-α-D-mannopyranosyl)-(1->6)-2-O-benzyl-4-O-methyl-β-D-mannopyranosid

There total 2 articles about Octyl-O-(2,3,4-tri-O-acetyl-6-desoxy-α-D-mannopyranosyl)-(1->6)-2-O-benzyl-4-O-methyl-β-D-mannopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

Octyl-2-O-benzyl-4-desoxy-β-D-lyxo-hexopyranosid (139494-04-5) + O-(2,3,4-Tri-O-acetyl-6-desoxy-α-D-mannopyranosyl)-trichloracetimidat (146683-30-9) → Octyl-O-(2,3,4-tri-O-acetyl-6-desoxy-α-D-mannopyranosyl)-(1->6)-2-O-benzyl-4-O-methyl-β-D-mannopyranosid (146597-65-1)

Guidance literature:

trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 ℃;

DOI:10.1016/S0040-4039(00)60178-8

Reference yield: 65.0%

Octyl-2-O-benzyl-4-O-methyl-β-D-mannopyranosid (139493-96-2) + O-(2,3,4-Tri-O-acetyl-6-desoxy-α-D-mannopyranosyl)-trichloracetimidat (146683-30-9) → Octyl-O-(2,3,4-tri-O-acetyl-6-desoxy-α-D-mannopyranosyl)-(1->6)-2-O-benzyl-4-O-methyl-β-D-mannopyranosid (146597-65-1)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; 3 A molecular sieve; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield: 76.0%

3,4,6-tri-O-acetyl-2-deoxy-2-acetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl trichloroacetimidate (126417-63-8) + Octyl-O-(2,3,4-tri-O-acetyl-6-desoxy-α-D-mannopyranosyl)-(1->6)-2-O-benzyl-4-O-methyl-β-D-mannopyranosid (146597-65-1) → Octyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-mannopyranosyl)-(1->3)-O-<(2,3,4-tri-O-acetyl-6-desoxy-α-D-mannopyranosyl)-(1->6)>-2-O-benzyl-4-O-methyl-β-D-mannopyranosid

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; 3 A molecular sieve; In dichloromethane; for 1h; Ambient temperature;

upstream raw materials:

Octyl-2-O-benzyl-4-desoxy-β-D-lyxo-hexopyranosid

O-(2,3,4-Tri-O-acetyl-6-desoxy-α-D-mannopyranosyl)-trichloracetimidat

Octyl-2-O-benzyl-4-O-methyl-β-D-mannopyranosid

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