(S)-2-(1,3-dioxoisoindolin-2-yl)-N-(2-oxo-2-phenylethyl)-3-phenylpropanamide

Base Information

Chemical Name:(S)-2-(1,3-dioxoisoindolin-2-yl)-N-(2-oxo-2-phenylethyl)-3-phenylpropanamide
CAS No.:872017-63-5
Molecular Formula:C₂₅H₂₀N₂O₄
Molecular Weight:412.445
Hs Code.:

Synonyms:(S)-2-(1,3-dioxoisoindolin-2-yl)-N-(2-oxo-2-phenylethyl)-3-phenylpropanamide

Suppliers and Price of (S)-2-(1,3-dioxoisoindolin-2-yl)-N-(2-oxo-2-phenylethyl)-3-phenylpropanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-(1,3-dioxoisoindolin-2-yl)-N-(2-oxo-2-phenylethyl)-3-phenylpropanamide

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Technology Process of (S)-2-(1,3-dioxoisoindolin-2-yl)-N-(2-oxo-2-phenylethyl)-3-phenylpropanamide

There total 1 articles about (S)-2-(1,3-dioxoisoindolin-2-yl)-N-(2-oxo-2-phenylethyl)-3-phenylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 613-89-8
2-Aminoacetophenone

: 5123-55-7
Nα-phthaloyl-L-phenylalanine

: 872017-63-5
(S)-2-(1,3-dioxoisoindolin-2-yl)-N-(2-oxo-2-phenylethyl)-3-phenylpropanamide

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; In pyridine; at 20 ℃; for 12h;

Reference yield: 41.0%

: 872017-63-5
(S)-2-(1,3-dioxoisoindolin-2-yl)-N-(2-oxo-2-phenylethyl)-3-phenylpropanamide

: 137349-42-9
(S)-2-(2-phenyl-1-(5-phenyloxazol-2-yl)ethyl)isoindoline-1,3-dione

Guidance literature:: With trichlorophosphate; In N,N-dimethyl-formamide; at 90 ℃; for 0.833333h; Inert atmosphere; Cooling with ice;
DOI:10.1021/jm5010607

Reference yield:

: 872017-63-5
(S)-2-(1,3-dioxoisoindolin-2-yl)-N-(2-oxo-2-phenylethyl)-3-phenylpropanamide

: 137349-43-0
(S)-2-phenyl-1-(5-phenyloxazol-2-yl)ethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / N,N-dimethyl-formamide / 0.83 h / 90 °C / Inert atmosphere; Cooling with ice

2: hydrazine / ethanol / 2 h / Inert atmosphere; Reflux

With hydrazine; trichlorophosphate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm5010607