Isopropyl 5-chloro-2-phenylpentanethioate

Base Information

Chemical Name:Isopropyl 5-chloro-2-phenylpentanethioate
CAS No.:152667-66-8
Molecular Formula:C₁₄H₁₉ClOS
Molecular Weight:270.823
Hs Code.:

Synonyms:Isopropyl 5-chloro-2-phenylpentanethioate

Suppliers and Price of Isopropyl 5-chloro-2-phenylpentanethioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Isopropyl 5-chloro-2-phenylpentanethioate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Isopropyl 5-chloro-2-phenylpentanethioate

There total 3 articles about Isopropyl 5-chloro-2-phenylpentanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 75-33-2
2-propanethiol

: 152667-63-5
(3-Chloropropyl)phenylacetyl chloride

: 152667-66-8
Isopropyl 5-chloro-2-phenylpentanethioate

Guidance literature:: With pyridine; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1021/jo00077a053

Reference yield:

: 103-82-2
phenylacetic acid

: 152667-66-8
Isopropyl 5-chloro-2-phenylpentanethioate

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / LDA / hexamethylphosphoric acid triamide; tetrahydrofuran / 1.) 0 deg C, 5 min; 50 deg C, 2 h, 2.) room temp., 3 h

2: oxalyl chloride / benzene / 1.) 0 deg C, 5 min, 2.) room temp., 3 h

3: 94 percent / pyridine / CH₂Cl₂ / 3 h / Ambient temperature

With pyridine; oxalyl dichloride; lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; benzene;
DOI:10.1021/jo00077a053

Reference yield:

: 152667-62-4
(3-Chloropropyl)phenyl acetic acid

: 152667-66-8
Isopropyl 5-chloro-2-phenylpentanethioate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride / benzene / 1.) 0 deg C, 5 min, 2.) room temp., 3 h

2: 94 percent / pyridine / CH₂Cl₂ / 3 h / Ambient temperature

With pyridine; oxalyl dichloride; In dichloromethane; benzene;
DOI:10.1021/jo00077a053