Carbonic acid 4-methoxy-2-((E)-6-methoxycarbonyloxy-3,7-dimethyl-octa-2,7-dienyl)-phenyl ester methyl ester

Base Information

Chemical Name:Carbonic acid 4-methoxy-2-((E)-6-methoxycarbonyloxy-3,7-dimethyl-octa-2,7-dienyl)-phenyl ester methyl ester
CAS No.:191401-67-9
Molecular Formula:C₂₁H₂₈O₇
Molecular Weight:392.449
Hs Code.:

Synonyms:Carbonic acid 4-methoxy-2-((E)-6-methoxycarbonyloxy-3,7-dimethyl-octa-2,7-dienyl)-phenyl ester methyl ester

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Chemical Property of Carbonic acid 4-methoxy-2-((E)-6-methoxycarbonyloxy-3,7-dimethyl-octa-2,7-dienyl)-phenyl ester methyl ester

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Technology Process of Carbonic acid 4-methoxy-2-((E)-6-methoxycarbonyloxy-3,7-dimethyl-octa-2,7-dienyl)-phenyl ester methyl ester

There total 5 articles about Carbonic acid 4-methoxy-2-((E)-6-methoxycarbonyloxy-3,7-dimethyl-octa-2,7-dienyl)-phenyl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 79-22-1
methyl chloroformate

: 191401-66-8
2-((E)-6-Hydroxy-3,7-dimethyl-octa-2,7-dienyl)-4-methoxy-phenol

: 191401-67-9
Carbonic acid 4-methoxy-2-((E)-6-methoxycarbonyloxy-3,7-dimethyl-octa-2,7-dienyl)-phenyl ester methyl ester

Guidance literature:: With pyridine; N,N-diethylaniline; In benzene; for 4h; Ambient temperature;

Reference yield:

: 6138-90-5
trans-geranyl bromide

: 191401-67-9
Carbonic acid 4-methoxy-2-((E)-6-methoxycarbonyloxy-3,7-dimethyl-octa-2,7-dienyl)-phenyl ester methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / Na / diethyl ether / 48 h / 36 °C

2: 65 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 0.25 h / -5 - 0 °C

3: 95 percent / Al(Oi-Pr)3 / toluene / 110 °C

4: 94 percent / diethylaniline, pyridine / benzene / 4 h / Ambient temperature

With pyridine; sodium; aluminum isopropoxide; 3-chloro-benzenecarboperoxoic acid; N,N-diethylaniline; In diethyl ether; dichloromethane; toluene; benzene;

Reference yield:

: 106-24-1
Geraniol

: 191401-67-9
Carbonic acid 4-methoxy-2-((E)-6-methoxycarbonyloxy-3,7-dimethyl-octa-2,7-dienyl)-phenyl ester methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / PBr₃ / diethyl ether / -20 °C

2: 82 percent / Na / diethyl ether / 48 h / 36 °C

3: 65 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 0.25 h / -5 - 0 °C

4: 95 percent / Al(Oi-Pr)3 / toluene / 110 °C

5: 94 percent / diethylaniline, pyridine / benzene / 4 h / Ambient temperature

With pyridine; sodium; phosphorus tribromide; aluminum isopropoxide; 3-chloro-benzenecarboperoxoic acid; N,N-diethylaniline; In diethyl ether; dichloromethane; toluene; benzene;