Thiophosphoric acid S-butyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Base Information

• Chemical Name: Thiophosphoric acid S-butyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester
• CAS No.: 143570-29-0
• Molecular Formula: C₄₅H₅₁O₈PS
• Molecular Weight: 782.935

Synonyms:Thiophosphoric acid S-butyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Chemical Property of Thiophosphoric acid S-butyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Chemical Property:

Purity/Quality:

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Technology Process of Thiophosphoric acid S-butyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

There total 1 articles about Thiophosphoric acid S-butyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

DL-2,3,4,5,6-penta-O-benzyl-myo-inositol (6195-45-5,13264-84-1,22132-86-1,25018-91-1,26277-05-4,28366-79-2,30694-52-1) + C10H27O3PSSi2 → Thiophosphoric acid S-butyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester (143570-29-0)

Guidance literature:

With pyridine; triisopropylbenzenesulfonyl chloride; triethylamine; for 24h; Yield given; Ambient temperature;

DOI:10.1016/S0040-4039(00)74812-X

Reference yield: 92.0%

Thiophosphoric acid S-butyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester (143570-29-0) → Thiophosphoric acid S-butyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl) ester (143599-65-9)

Guidance literature:

With boron trifluoride diethyl etherate; ethanethiol; In chloroform;

DOI:10.1016/S0040-4039(00)74812-X

upstream raw materials:

DL-2,3,4,5,6-penta-O-benzyl-myo-inositol

Downstream raw materials:

Thiophosphoric acid S-butyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl) ester

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