[(2S,3S)-1-(tert-butoxycarbonyl)-3-(4-methoxy-3-vinylphenoxy)prolyl]isoleucinamide

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Chemical Name:[(2S,3S)-1-(tert-butoxycarbonyl)-3-(4-methoxy-3-vinylphenoxy)prolyl]isoleucinamide
CAS No.:1009839-34-2
Molecular Formula:C₂₅H₃₇N₃O₆
Molecular Weight:475.585
Hs Code.:

Synonyms:[(2S,3S)-1-(tert-butoxycarbonyl)-3-(4-methoxy-3-vinylphenoxy)prolyl]isoleucinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [(2S,3S)-1-(tert-butoxycarbonyl)-3-(4-methoxy-3-vinylphenoxy)prolyl]isoleucinamide

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Technology Process of [(2S,3S)-1-(tert-butoxycarbonyl)-3-(4-methoxy-3-vinylphenoxy)prolyl]isoleucinamide

There total 3 articles about [(2S,3S)-1-(tert-butoxycarbonyl)-3-(4-methoxy-3-vinylphenoxy)prolyl]isoleucinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1009839-40-0
(2S,3S)-[1-tert-butoxycarbonyl-3-(4-methoxy-3-vinylphenoxy)prolyl]-isoleucine-vinylamide

: 929896-08-2
C₂₅H₃₅N₃O₆

: 1009839-34-2
[(2S,3S)-1-(tert-butoxycarbonyl)-3-(4-methoxy-3-vinylphenoxy)prolyl]isoleucinamide

Guidance literature:: Grubbs catalyst first generation; In 1,2-dichloro-ethane; for 24h; Heating;
DOI:10.1021/jo702092x

Reference yield: 71.0%

: L-isoleucinamide acetic acid salt

: 1009839-26-2
(2S,3S)-1-tert-butoxycarbonyl-2-formyl-3-(4-methoxy-3-vinylphenoxy)pyrrolidine

: 1009839-34-2
[(2S,3S)-1-(tert-butoxycarbonyl)-3-(4-methoxy-3-vinylphenoxy)prolyl]isoleucinamide

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1002/ejoc.200900122