1,2-bis[6-(3,5-dimethoxy)phenyl-2-methyl-1-benzothiophen-3-yl]perfluorocyclopentene

Base Information

• Chemical Name: 1,2-bis[6-(3,5-dimethoxy)phenyl-2-methyl-1-benzothiophen-3-yl]perfluorocyclopentene
• CAS No.: 1100161-08-7
• Molecular Formula: C₃₉H₃₀F₆O₄S₂
• Molecular Weight: 740.787

Synonyms:1,2-bis[6-(3,5-dimethoxy)phenyl-2-methyl-1-benzothiophen-3-yl]perfluorocyclopentene

Chemical Property of 1,2-bis[6-(3,5-dimethoxy)phenyl-2-methyl-1-benzothiophen-3-yl]perfluorocyclopentene

Chemical Property:

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Technology Process of 1,2-bis[6-(3,5-dimethoxy)phenyl-2-methyl-1-benzothiophen-3-yl]perfluorocyclopentene

There total 1 articles about 1,2-bis[6-(3,5-dimethoxy)phenyl-2-methyl-1-benzothiophen-3-yl]perfluorocyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

3,5-dimethoxyphenylboronic acid (192182-54-0) + 1,2-bis(6-iodo-2-methylbenzothiophen-3-yl)-3,3,4,4,5,5-hexafluorocyclopentene (167890-07-5) → 1,2-bis[6-(3,5-dimethoxy)phenyl-2-methyl-1-benzothiophen-3-yl]perfluorocyclopentene (1100161-08-7)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; Inert atmosphere;

DOI:10.1039/b810955a

Reference yield: 89.0%

1,2-bis[6-(3,5-dimethoxy)phenyl-2-methyl-1-benzothiophen-3-yl]perfluorocyclopentene (1100161-08-7) → 1,2-bis[6-(3,5-dihydroxy)phenyl-2-methyl-1-benzothiophen-3-yl]perfluorocyclopentene (1100161-09-8)

Guidance literature:

With boron tribromide; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1039/b810955a

upstream raw materials:

3,5-dimethoxyphenylboronic acid

1,2-bis(6-iodo-2-methylbenzothiophen-3-yl)-3,3,4,4,5,5-hexafluorocyclopentene

Downstream raw materials:

1,2-bis[6-(3,5-dihydroxy)phenyl-2-methyl-1-benzothiophen-3-yl]perfluorocyclopentene

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