methyl (2R)-<(3S,4R)-4-(benzothiazol-2-yldithio)-2-oxo-3-phenylacetamidoazetidin-1-yl>-3-methylbut-3-enoate

Base Information

Chemical Name:methyl (2R)-<(3S,4R)-4-(benzothiazol-2-yldithio)-2-oxo-3-phenylacetamidoazetidin-1-yl>-3-methylbut-3-enoate
CAS No.:62284-24-6
Molecular Formula:C₂₄H₂₃N₃O₄S₃
Molecular Weight:513.662
Hs Code.:

Synonyms:methyl (2R)-<(3S,4R)-4-(benzothiazol-2-yldithio)-2-oxo-3-phenylacetamidoazetidin-1-yl>-3-methylbut-3-enoate

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Chemical Property of methyl (2R)-<(3S,4R)-4-(benzothiazol-2-yldithio)-2-oxo-3-phenylacetamidoazetidin-1-yl>-3-methylbut-3-enoate

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Technology Process of methyl (2R)-<(3S,4R)-4-(benzothiazol-2-yldithio)-2-oxo-3-phenylacetamidoazetidin-1-yl>-3-methylbut-3-enoate

There total 1 articles about methyl (2R)-<(3S,4R)-4-(benzothiazol-2-yldithio)-2-oxo-3-phenylacetamidoazetidin-1-yl>-3-methylbut-3-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24652-72-0
methyl 6β-(phenylacetamido)penicillanate 1β-oxide

: 149-30-4,118090-09-8
2-Mercaptobenzothiazole

: 62284-24-6
methyl (2R)-<(3S,4R)-4-(benzothiazol-2-yldithio)-2-oxo-3-phenylacetamidoazetidin-1-yl>-3-methylbut-3-enoate

Guidance literature:: In toluene; for 4h; Heating;
DOI:10.1021/ja00457a032

Reference yield: 72.0%

: 62284-24-6
methyl (2R)-<(3S,4R)-4-(benzothiazol-2-yldithio)-2-oxo-3-phenylacetamidoazetidin-1-yl>-3-methylbut-3-enoate

: (S)-2-[(2R,3R)-2-(Benzothiazol-2-yldisulfanyl)-4-oxo-3-phenylacetylamino-azetidin-1-yl]-3,4-dichloro-3-methyl-butyric acid methyl ester

: 57892-26-9
(2S,3R,5R,6R)-3-Chloromethyl-3-methyl-7-oxo-6-phenylacetylamino-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid methyl ester

Guidance literature:: With sodium chloride; In dichloromethane; water; at 25 ℃; Pt electrodes, 10 mA/cm2;
DOI:10.1246/cl.1982.1829

Reference yield: 72.0%

: 62284-24-6
methyl (2R)-<(3S,4R)-4-(benzothiazol-2-yldithio)-2-oxo-3-phenylacetamidoazetidin-1-yl>-3-methylbut-3-enoate

: 93061-18-8
(2S,5R,6R)-3-Chloromethyl-3-methyl-7-oxo-6-phenylacetylamino-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid methyl ester

: (S)-2-[(2R,3R)-2-(Benzothiazol-2-yldisulfanyl)-4-oxo-3-phenylacetylamino-azetidin-1-yl]-3,4-dichloro-3-methyl-butyric acid methyl ester

Guidance literature:: With sodium chloride; In dichloromethane; water; at 23 - 27 ℃; electrolysis, Pt electrodes, 10 mA/cm²;
DOI:10.1002/bscb.19820911202