2-(3-(4-chlorophenyl)-3-oxoprop-1-enyl)-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indol-4-one

Base Information

• Chemical Name: 2-(3-(4-chlorophenyl)-3-oxoprop-1-enyl)-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indol-4-one
• CAS No.: 1437785-46-0
• Molecular Formula: C₁₉H₁₈ClNO₂
• Molecular Weight: 327.81

Synonyms:2-(3-(4-chlorophenyl)-3-oxoprop-1-enyl)-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indol-4-one

Chemical Property of 2-(3-(4-chlorophenyl)-3-oxoprop-1-enyl)-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indol-4-one

Chemical Property:

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Technology Process of 2-(3-(4-chlorophenyl)-3-oxoprop-1-enyl)-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indol-4-one

There total 1 articles about 2-(3-(4-chlorophenyl)-3-oxoprop-1-enyl)-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indol-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.5%

6,6-dimethyl-4-oxo-4,5,6,7-tetrahydro-1H-indole-2-carbaldehyde (13265-93-5) + para-chloroacetophenone (99-91-2) → 2-(3-(4-chlorophenyl)-3-oxoprop-1-enyl)-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indol-4-one (1437785-46-0)

Guidance literature:

With potassium hydroxide; In ethanol; at 20 ℃; for 5h;

DOI:10.3390/molecules18032683

Reference yield: 87.5%

2-(3-(4-chlorophenyl)-3-oxoprop-1-enyl)-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indol-4-one (1437785-46-0) + 4-aminosulfonylphenylhydrazine (4392-54-5) → 4-(3-(4-chlorophenyl)-5-(6,6-dimethyl-4-oxo-4,5,6,7-tetrahydro-1H-indol-2-yl)-4,5-dihydro-1H-pyrazol-1-yl)benzenesulfonamide

Guidance literature:

In methanol; for 6h; Reflux;

DOI:10.3390/molecules18032683

Reference yield: 82.3%

3-hydrazinyl-5,10-dihydro-[1,2,4]triazino[5,6-b]quinoxaline (1437785-65-3) + 2-(3-(4-chlorophenyl)-3-oxoprop-1-enyl)-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indol-4-one (1437785-46-0) → 2-(3-(4-chlorophenyl)-1-(5,10-Dihydro-[1,2,4]triazino[5,6-b]quinoxalin-3-yl)-1H-pyrazol-5-yl)-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indol-4-one (1437785-83-5)

Guidance literature:

With acetic acid; In ethanol; for 7h; Reflux;

DOI:10.3390/molecules18032683

upstream raw materials:

6,6-dimethyl-4-oxo-4,5,6,7-tetrahydro-1H-indole-2-carbaldehyde

para-chloroacetophenone

Downstream raw materials:

2-(3-(4-chlorophenyl)-1-(5,10-Dihydro-[1,2,4]triazino[5,6-b]quinoxalin-3-yl)-1H-pyrazol-5-yl)-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indol-4-one

3-(4-chlorophenyl)-5-(6,6-dimethyl-4-oxo-4,5,6,7-tetrahydro-1H-indol-2-yl)-4,5-dihydro-1H-pyrazole-1-carbothioamide

2-(3-(4-chlorophenyl)-4,5-dihydro-1H-pyrazol-5-yl)-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indol-4-one

2-(3-(4-chlorophenyl)-4,5-dihydroisoxazol-5-yl)-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indol-4-one

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