1,5,6,10b-tetrahydro-9-methoxy-10b-<(3,4-dimethoxyphenyl)methyl>-8-metoxypyrrolo<2,1-a>isoquinolin-3-(2H)-one

Base Information

Chemical Name:1,5,6,10b-tetrahydro-9-methoxy-10b-<(3,4-dimethoxyphenyl)methyl>-8-metoxypyrrolo<2,1-a>isoquinolin-3-(2H)-one
CAS No.:110698-47-0
Molecular Formula:C₂₂H₂₅NO₅
Molecular Weight:383.444
Hs Code.:

Synonyms:1,5,6,10b-tetrahydro-9-methoxy-10b-<(3,4-dimethoxyphenyl)methyl>-8-metoxypyrrolo<2,1-a>isoquinolin-3-(2H)-one

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Chemical Property of 1,5,6,10b-tetrahydro-9-methoxy-10b-<(3,4-dimethoxyphenyl)methyl>-8-metoxypyrrolo<2,1-a>isoquinolin-3-(2H)-one

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Technology Process of 1,5,6,10b-tetrahydro-9-methoxy-10b-<(3,4-dimethoxyphenyl)methyl>-8-metoxypyrrolo<2,1-a>isoquinolin-3-(2H)-one

There total 4 articles about 1,5,6,10b-tetrahydro-9-methoxy-10b-<(3,4-dimethoxyphenyl)methyl>-8-metoxypyrrolo<2,1-a>isoquinolin-3-(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 110698-46-9
1,5,6,10b-tetrahydro-8-methoxy-10b-<(3,4-dimethoxyphenyl)methyl>-9-(phenylmethoxy)pyrrolo<2,1-a>isoquinolin-3(2H)-one

: 110698-47-0
1,5,6,10b-tetrahydro-9-methoxy-10b-<(3,4-dimethoxyphenyl)methyl>-8-metoxypyrrolo<2,1-a>isoquinolin-3-(2H)-one

Guidance literature:: With dibenzyl ether; hydrogen; palladium on activated charcoal; In ethanol; ethyl acetate; for 12h;
DOI:10.1021/jo00235a004

Reference yield:

: 22231-61-4
2-[4-(benzyloxy)-3-methoxyphenyl]ethylamine

: 110698-47-0
1,5,6,10b-tetrahydro-9-methoxy-10b-<(3,4-dimethoxyphenyl)methyl>-8-metoxypyrrolo<2,1-a>isoquinolin-3-(2H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: 2.) AcCl / 1.) CH₂Cl₂, RT, 116 h, 2.) CH₂Cl₂, reflux, 48.5 h

2: 29 percent / CH₂Cl₂ / 0.75 h

3: 100 percent / formic acid / CH₂Cl₂ / 0.17 h

4: 100 percent / H₂,benzyl ether / 5percent Pd/C / ethyl acetate; ethanol / 12 h

With formic acid; dibenzyl ether; hydrogen; acetyl chloride; palladium on activated charcoal; In ethanol; dichloromethane; ethyl acetate;
DOI:10.1021/jo00235a004

Reference yield:

: 110698-41-4
N-<2-(4-(benzyloksy)-3-metoxyphenyl)ethyl>succinimide

: 110698-47-0
1,5,6,10b-tetrahydro-9-methoxy-10b-<(3,4-dimethoxyphenyl)methyl>-8-metoxypyrrolo<2,1-a>isoquinolin-3-(2H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 29 percent / CH₂Cl₂ / 0.75 h

2: 100 percent / formic acid / CH₂Cl₂ / 0.17 h

3: 100 percent / H₂,benzyl ether / 5percent Pd/C / ethyl acetate; ethanol / 12 h

With formic acid; dibenzyl ether; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; ethyl acetate;
DOI:10.1021/jo00235a004