1,4-dideutero-threo-2,3-dibenzylbutane

Base Information

• Chemical Name: 1,4-dideutero-threo-2,3-dibenzylbutane
• CAS No.: 136934-54-8
• Molecular Formula: C₁₈H₂₂
• Molecular Weight: 240.357

Synonyms:1,4-dideutero-threo-2,3-dibenzylbutane

Chemical Property of 1,4-dideutero-threo-2,3-dibenzylbutane

Chemical Property:

Purity/Quality:

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Technology Process of 1,4-dideutero-threo-2,3-dibenzylbutane

There total 6 articles about 1,4-dideutero-threo-2,3-dibenzylbutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

allylbenzene (300-57-2,57807-91-7) → 1-phenylpropene (637-50-3) + C18H19(2)H + 1‐[2H]‐3‐phenylpropane (117657-84-8) + 1,4-dideutero-threo-2,3-dibenzylbutane (136934-54-8)

Guidance literature:

allylbenzene; With zirconocene dichloride; diethylaluminium chloride; magnesium; In tetrahydrofuran; at 0 - 22 ℃; for 72h; Inert atmosphere; Schlenk technique;

With hydrogen chloride; In tetrahydrofuran; water-d2; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.jorganchem.2014.09.033

Reference yield:

allylbenzene (300-57-2,57807-91-7) → 1-phenylpropene (637-50-3) + C18H20(2)H2 + C18H19(2)H + 1‐[2H]‐3‐phenylpropane (117657-84-8) + 1,4-dideutero-threo-2,3-dibenzylbutane (136934-54-8)

Guidance literature:

allylbenzene; With cyclopentadienylzirconium trichloride; ethylaluminum dichloride; magnesium; In tetrahydrofuran; at 0 - 22 ℃; for 72h; Inert atmosphere; Schlenk technique;

With hydrogen chloride; In tetrahydrofuran; water-d2; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.jorganchem.2014.09.033

Reference yield:

allylbenzene (300-57-2,57807-91-7) → C18H20(2)H2 + 1,4-dideutero-threo-2,3-dibenzylbutane (136934-54-8)

Guidance literature:

allylbenzene; With rac-dimethylsilylenebis(indenyl)zirconium dichloride; ethylaluminum dichloride; magnesium; In tetrahydrofuran; at 0 - 22 ℃; for 72h; Inert atmosphere; Schlenk technique;

With hydrogen chloride; In tetrahydrofuran; water-d2; Reagent/catalyst; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.jorganchem.2014.09.033

upstream raw materials:

allylbenzene

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