3-benzyloxycarbonyl-7-benzyloxymethyl-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-9-carbonsaeurepentafuorophenylester

Base Information

Chemical Name:3-benzyloxycarbonyl-7-benzyloxymethyl-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-9-carbonsaeurepentafuorophenylester
CAS No.:116171-87-0
Molecular Formula:C₃₉H₃₅F₅N₂O₅
Molecular Weight:706.709
Hs Code.:

Synonyms:3-benzyloxycarbonyl-7-benzyloxymethyl-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-9-carbonsaeurepentafuorophenylester

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Chemical Property of 3-benzyloxycarbonyl-7-benzyloxymethyl-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-9-carbonsaeurepentafuorophenylester

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Technology Process of 3-benzyloxycarbonyl-7-benzyloxymethyl-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-9-carbonsaeurepentafuorophenylester

There total 10 articles about 3-benzyloxycarbonyl-7-benzyloxymethyl-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-9-carbonsaeurepentafuorophenylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 116171-86-9
3-benzyloxycarbonyl-7-benzyloxymethyl-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-9-carbonsaeure

: 116171-87-0
3-benzyloxycarbonyl-7-benzyloxymethyl-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-9-carbonsaeurepentafuorophenylester

Guidance literature:: With dicyclohexyl-carbodiimide; In ethyl acetate; for 15h; Ambient temperature;
DOI:10.1016/S0040-4020(01)86863-0

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 116171-87-0
3-benzyloxycarbonyl-7-benzyloxymethyl-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-9-carbonsaeurepentafuorophenylester

Guidance literature:: Multi-step reaction with 7 steps

1: anhydrous sodium carbonate / tetrahydrofuran / 16 h / 50 °C

2: 98 percent / pyridine / 1 h / 40 °C

3: 98 percent / tetra-n-butyl ammonium bromide, sodium iodide / toluene / 2 h / Heating

4: 90 percent / sodium hydroxide, 30percent hydrogen peroxide / ethanol / 3 h / Ambient temperature

5: 77 percent / Amberlyst 15 / 120 h / 60 °C

6: sodium hydroxide, water, ethyl acetate, HCl / ethanol / 100 h / 100 °C

7: 95 percent / dicyclohexylcarbodiimide / ethyl acetate / 15 h / Ambient temperature

With pyridine; hydrogenchloride; sodium hydroxide; Amberlyst 15; tetrabutylammomium bromide; water; dihydrogen peroxide; sodium carbonate; ethyl acetate; dicyclohexyl-carbodiimide; sodium iodide; In tetrahydrofuran; ethanol; ethyl acetate; toluene;
DOI:10.1016/S0040-4020(01)86863-0

Reference yield:

: 107688-23-3
2-benzyloxymethyl-2,3,4,5,6,7,8,13,13b-octahydro-1H-azepino<1',2':1,2>pyrido<3,4-b>indol

: 116171-87-0
3-benzyloxycarbonyl-7-benzyloxymethyl-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-9-carbonsaeurepentafuorophenylester

Guidance literature:: Multi-step reaction with 7 steps

1: anhydrous sodium carbonate / tetrahydrofuran / 16 h / 50 °C

2: 98 percent / pyridine / 1 h / 40 °C

3: 98 percent / tetra-n-butyl ammonium bromide, sodium iodide / toluene / 2 h / Heating

4: 90 percent / sodium hydroxide, 30percent hydrogen peroxide / ethanol / 3 h / Ambient temperature

5: 77 percent / Amberlyst 15 / 120 h / 60 °C

6: sodium hydroxide, water, ethyl acetate, HCl / ethanol / 100 h / 100 °C

7: 95 percent / dicyclohexylcarbodiimide / ethyl acetate / 15 h / Ambient temperature

With pyridine; hydrogenchloride; sodium hydroxide; Amberlyst 15; tetrabutylammomium bromide; water; dihydrogen peroxide; sodium carbonate; ethyl acetate; dicyclohexyl-carbodiimide; sodium iodide; In tetrahydrofuran; ethanol; ethyl acetate; toluene;
DOI:10.1016/S0040-4020(01)86863-0