N-[(1R,2R)-2-(3-cyclohexa-1,4-dienylpropylamino)-1,2-diphenylethyl]-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-[(1R,2R)-2-(3-cyclohexa-1,4-dienylpropylamino)-1,2-diphenylethyl]-4-methylbenzenesulfonamide
CAS No.:851051-44-0
Molecular Formula:C₃₀H₃₄N₂O₂S
Molecular Weight:486.678
Hs Code.:

Synonyms:N-[(1R,2R)-2-(3-cyclohexa-1,4-dienylpropylamino)-1,2-diphenylethyl]-4-methylbenzenesulfonamide

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Chemical Property of N-[(1R,2R)-2-(3-cyclohexa-1,4-dienylpropylamino)-1,2-diphenylethyl]-4-methylbenzenesulfonamide

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Technology Process of N-[(1R,2R)-2-(3-cyclohexa-1,4-dienylpropylamino)-1,2-diphenylethyl]-4-methylbenzenesulfonamide

There total 4 articles about N-[(1R,2R)-2-(3-cyclohexa-1,4-dienylpropylamino)-1,2-diphenylethyl]-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.9%

: 167316-27-0
N-[(1S,2S)-2-amino-1,2-diphenylethyl]-4-methylbenzenesulfonamide

: 87151-66-4
3-(cyclohexa-1,4-dien-1-yl)propan-1-ol

: 851051-44-0,851051-41-7
N-[(1R,2R)-2-(3-cyclohexa-1,4-dienylpropylamino)-1,2-diphenylethyl]-4-methylbenzenesulfonamide

Guidance literature:: 3-(cyclohexa-1,4-dien-1-yl)propan-1-ol; With 2,6-dimethylpyridine; at 0 ℃; for 0.5h; Inert atmosphere;

With trifluoromethylsulfonic anhydride; at 0 - 20 ℃; for 1.5h; Inert atmosphere;

N-[(1S,2S)-2-amino-1,2-diphenylethyl]-4-methylbenzenesulfonamide; With triethylamine; In dichloromethane; at 0 ℃; for 1h; Reagent/catalyst; Inert atmosphere;

Reference yield:

: C₃₀H₃₂N₂O₂S

: 851051-44-0,851051-41-7
N-[(1R,2R)-2-(3-cyclohexa-1,4-dienylpropylamino)-1,2-diphenylethyl]-4-methylbenzenesulfonamide

Guidance literature:: With sodium cyanoborohydride; In methanol; for 48h; Inert atmosphere;
DOI:10.1039/c1ob05208j

Reference yield:

: 144222-34-4
(R,R)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine

: 851051-44-0,851051-41-7
N-[(1R,2R)-2-(3-cyclohexa-1,4-dienylpropylamino)-1,2-diphenylethyl]-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / methanol / 2.5 h / Molecular sieve; Inert atmosphere

2: sodium cyanoborohydride / methanol / 48 h / Inert atmosphere

With sodium cyanoborohydride; acetic acid; In methanol;
DOI:10.1039/c1ob05208j