toluene-4-thiosulfonic acid S-(2-amino-5-tert-butyl-benzothiazol-6-yl)ester

Base Information

Chemical Name:toluene-4-thiosulfonic acid S-(2-amino-5-tert-butyl-benzothiazol-6-yl)ester
CAS No.:261709-46-0
Molecular Formula:C₁₈H₂₀N₂O₂S₃
Molecular Weight:392.567
Hs Code.:

Synonyms:toluene-4-thiosulfonic acid S-(2-amino-5-tert-butyl-benzothiazol-6-yl)ester

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Chemical Property of toluene-4-thiosulfonic acid S-(2-amino-5-tert-butyl-benzothiazol-6-yl)ester

Chemical Property:

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Technology Process of toluene-4-thiosulfonic acid S-(2-amino-5-tert-butyl-benzothiazol-6-yl)ester

There total 5 articles about toluene-4-thiosulfonic acid S-(2-amino-5-tert-butyl-benzothiazol-6-yl)ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1950-69-2
toluene-p-sulfonyl bromide

: 261709-31-3
2-amino-5-tert-butyl-benzothiazole-6-thiol

: 261709-46-0
toluene-4-thiosulfonic acid S-(2-amino-5-tert-butyl-benzothiazol-6-yl)ester

Guidance literature:: With pyridine; In ethyl acetate; for 6h;
DOI:10.1016/S0040-4039(00)00591-8

Reference yield:

: 3972-65-4
1-bromo-4-tert-butylbenzene

: 261709-46-0
toluene-4-thiosulfonic acid S-(2-amino-5-tert-butyl-benzothiazol-6-yl)ester

Guidance literature:: Multi-step reaction with 5 steps

1: 60 percent / HNO₃; H₂SO₄ / acetic anhydride

2: 95 percent / H₂ / Raney nickel

3: 75 percent / NaBr; Bromine / methanol

4: dithiothreitol; K₂HPO₄ buffer / ethanol / 16 h / Heating

5: pyridine / ethyl acetate / 6 h

With pyridine; K₂HPO₄ buffer; sulfuric acid; hydrogen; bromine; nitric acid; sodium bromide; diothiothreitol; nickel; In methanol; ethanol; acetic anhydride; ethyl acetate; 1: Nitration / 2: Reduction / 3: Cyclization / 4: Reduction / 5: Tosylation;
DOI:10.1016/S0040-4039(00)00591-8

Reference yield:

: 70729-05-4
1-Bromo-4-tert-butyl-2-nitro-benzene

: 261709-46-0
toluene-4-thiosulfonic acid S-(2-amino-5-tert-butyl-benzothiazol-6-yl)ester

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / H₂ / Raney nickel

2: 75 percent / NaBr; Bromine / methanol

3: dithiothreitol; K₂HPO₄ buffer / ethanol / 16 h / Heating

4: pyridine / ethyl acetate / 6 h

With pyridine; K₂HPO₄ buffer; hydrogen; bromine; sodium bromide; diothiothreitol; nickel; In methanol; ethanol; ethyl acetate; 1: Reduction / 2: Cyclization / 3: Reduction / 4: Tosylation;
DOI:10.1016/S0040-4039(00)00591-8