4-methyl-N-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)benzenesulfonamide

Base Information

Chemical Name:4-methyl-N-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)benzenesulfonamide
CAS No.:22360-51-6
Molecular Formula:C₁₄H₁₂N₄O₃S
Molecular Weight:316.34
Hs Code.:
Mol file:22360-51-6.mol

Synonyms:3-<(p-tolylsulfonyl)amino>-1,2,3-benzotriazin-4(3H)-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methyl-N-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)benzenesulfonamide

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Technology Process of 4-methyl-N-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)benzenesulfonamide

There total 6 articles about 4-methyl-N-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 92376-36-8
1-anthraniloyl-2-(p-tolylsulfonyl)hydrazine

: 22360-51-6
3-<(p-tolylsulfonyl)amino>-1,2,3-benzotriazin-4(3H)-one

Guidance literature:: With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 0.25h;
DOI:10.1021/jo00236a047

Reference yield: 62.0%

: 111635-82-6
3--1,2,3-benzotriazin-4-(3H)-one

: 22360-51-6
3-<(p-tolylsulfonyl)amino>-1,2,3-benzotriazin-4(3H)-one

Guidance literature:: With sodium methylate; In methanol; at 40 ℃; for 0.333333h;
DOI:10.1021/jo00236a047

Reference yield:

: 41225-81-4
3-amino-1,2,3-benzotriazin-4(3H)-one

: 22360-51-6
3-<(p-tolylsulfonyl)amino>-1,2,3-benzotriazin-4(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / pyridine / 3 h / 25 °C

2: 62 percent / sodium methoxide / methanol / 0.33 h / 40 °C

With sodium methylate; In pyridine; methanol;
DOI:10.1021/jo00236a047