N-[2-[(2,6-dichloropyrimidin-4-yl)amino]phenyl]-2,2-difluoro-acetamide

Base Information

Chemical Name:N-[2-[(2,6-dichloropyrimidin-4-yl)amino]phenyl]-2,2-difluoro-acetamide
CAS No.:1010697-29-6
Molecular Formula:C₁₂H₈Cl₂F₂N₄O
Molecular Weight:333.125
Hs Code.:

Synonyms:N-[2-[(2,6-dichloropyrimidin-4-yl)amino]phenyl]-2,2-difluoro-acetamide

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Chemical Property of N-[2-[(2,6-dichloropyrimidin-4-yl)amino]phenyl]-2,2-difluoro-acetamide

Chemical Property:

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Technology Process of N-[2-[(2,6-dichloropyrimidin-4-yl)amino]phenyl]-2,2-difluoro-acetamide

There total 4 articles about N-[2-[(2,6-dichloropyrimidin-4-yl)amino]phenyl]-2,2-difluoro-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3764-01-0
2,4,6-trichloropyrimidine

: 1010697-30-9
2,2-difluoro-N-(2-nitrophenyl)acetamide

: 1010697-29-6
N-[2-[(2,6-dichloropyrimidin-4-yl)amino]phenyl]-2,2-difluoro-acetamide

Guidance literature:: 2,2-difluoro-N-(2-nitrophenyl)acetamide; With hydrogen; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In ethyl acetate; under 750.075 Torr; Asynt Technologies H-Cube;

2,4,6-trichloropyrimidine; In N,N-dimethyl acetamide; at 20 ℃; for 64h;

Reference yield:

: 3764-01-0
2,4,6-trichloropyrimidine

: 70057-41-9
C₈H₈F₂N₂O

: 1010697-29-6
N-[2-[(2,6-dichloropyrimidin-4-yl)amino]phenyl]-2,2-difluoro-acetamide

Guidance literature:: In N,N-dimethyl acetamide; at 20 ℃; for 64h;

Reference yield:

: 88-74-4
2-nitro-aniline

: 1010697-29-6
N-[2-[(2,6-dichloropyrimidin-4-yl)amino]phenyl]-2,2-difluoro-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: zirconium(IV) chloride / 0.17 h / 90 - 103 °C

2: hydrogen; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / ethyl acetate / 750.08 Torr

3: N,N-dimethyl acetamide / 64 h / 20 °C

With hydrogen; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; zirconium(IV) chloride; In N,N-dimethyl acetamide; ethyl acetate;