8-{3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]phenyl}-9H-purine

Base Information

Chemical Name:8-{3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]phenyl}-9H-purine
CAS No.:915949-10-9
Molecular Formula:C₂₂H₂₀N₄O₃
Molecular Weight:388.426
Hs Code.:

Synonyms:8-{3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]phenyl}-9H-purine

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Chemical Property of 8-{3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]phenyl}-9H-purine

Chemical Property:

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Technology Process of 8-{3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]phenyl}-9H-purine

There total 4 articles about 8-{3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]phenyl}-9H-purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13754-19-3
4,5-pyrimidinediamine

: 915771-21-0
3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]benzoic acid

: 915949-10-9
8-{3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]phenyl}-9H-purine

Guidance literature:: With 1,1-Carbodiimide; In propyl cyanide; at 20 - 200 ℃; for 2h; Microwave irradiation;

Reference yield:

: 915771-22-1
methyl 3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]benzoate

: 915949-10-9
8-{3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]phenyl}-9H-purine

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hydroxide; water / tetrahydrofuran / 72 h / 20 °C

1.2: pH 3

2.1: 1,1-Carbodiimide / propyl cyanide / 2 h / 20 - 200 °C / Microwave irradiation

With lithium hydroxide; water; In tetrahydrofuran; propyl cyanide;

Reference yield:

: 54915-31-0
methyl 3-(benzyloxy)-5-hydroxybenzoate

: 915949-10-9
8-{3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]phenyl}-9H-purine

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / propyl cyanide / 3 h / 130 °C

2.1: lithium hydroxide; water / tetrahydrofuran / 72 h / 20 °C

2.2: pH 3

3.1: 1,1-Carbodiimide / propyl cyanide / 2 h / 20 - 200 °C / Microwave irradiation

With lithium hydroxide; water; potassium carbonate; In tetrahydrofuran; propyl cyanide;