4-(2-(3-carboxy-4-hydroxyphenyl)-2-oxoethoxy)-4-oxobutan-1-aminium-2,2,2-trifluoroacetate

Base Information

Chemical Name:4-(2-(3-carboxy-4-hydroxyphenyl)-2-oxoethoxy)-4-oxobutan-1-aminium-2,2,2-trifluoroacetate
CAS No.:1292298-77-1
Molecular Formula:C₂HF₃O₂*C₁₃H₁₅NO₆
Molecular Weight:395.289
Hs Code.:

Synonyms:4-(2-(3-carboxy-4-hydroxyphenyl)-2-oxoethoxy)-4-oxobutan-1-aminium-2,2,2-trifluoroacetate

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Chemical Property of 4-(2-(3-carboxy-4-hydroxyphenyl)-2-oxoethoxy)-4-oxobutan-1-aminium-2,2,2-trifluoroacetate

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Technology Process of 4-(2-(3-carboxy-4-hydroxyphenyl)-2-oxoethoxy)-4-oxobutan-1-aminium-2,2,2-trifluoroacetate

There total 4 articles about 4-(2-(3-carboxy-4-hydroxyphenyl)-2-oxoethoxy)-4-oxobutan-1-aminium-2,2,2-trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1292299-08-1
5-(2-(4-(tert-butoxycarbonylamino)butanoyloxy)acetyl)-2-hydroxybenzoic acid

: 76-05-1
trifluoroacetic acid

: 1292298-77-1
4-(2-(3-carboxy-4-hydroxyphenyl)-2-oxoethoxy)-4-oxobutan-1-aminium-2,2,2-trifluoroacetate

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1139/V10-143

Reference yield:

: 1292299-06-9
benzyl 5-acetyl-2-(benzyloxy)benzoate

: 1292298-77-1
4-(2-(3-carboxy-4-hydroxyphenyl)-2-oxoethoxy)-4-oxobutan-1-aminium-2,2,2-trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1: phenyltrimethylammonium tribromide / methanol; dichloromethane / 20 °C

2: potassium carbonate / acetonitrile / 20 °C

3: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 °C

4: dichloromethane / 20 °C

With palladium 10% on activated carbon; hydrogen; phenyltrimethylammonium tribromide; potassium carbonate; In methanol; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1139/V10-143

Reference yield:

: 943969-36-6
benzyl 2-(benzyloxy)-5-(2-bromoacetyl)benzoate

: 1292298-77-1
4-(2-(3-carboxy-4-hydroxyphenyl)-2-oxoethoxy)-4-oxobutan-1-aminium-2,2,2-trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 20 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 °C

3: dichloromethane / 20 °C

With palladium 10% on activated carbon; hydrogen; potassium carbonate; In dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1139/V10-143