(Z)-3,7-anhydro-4,5,6,8-tetra-O-benzyl-2-deoxy-D-gluco-oct-2-enonic acid methyl ester

Base Information

Chemical Name:(Z)-3,7-anhydro-4,5,6,8-tetra-O-benzyl-2-deoxy-D-gluco-oct-2-enonic acid methyl ester
CAS No.:493018-20-5
Molecular Formula:C₃₇H₃₈O₇
Molecular Weight:594.705
Hs Code.:

Synonyms:(Z)-3,7-anhydro-4,5,6,8-tetra-O-benzyl-2-deoxy-D-gluco-oct-2-enonic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-3,7-anhydro-4,5,6,8-tetra-O-benzyl-2-deoxy-D-gluco-oct-2-enonic acid methyl ester

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Technology Process of (Z)-3,7-anhydro-4,5,6,8-tetra-O-benzyl-2-deoxy-D-gluco-oct-2-enonic acid methyl ester

There total 1 articles about (Z)-3,7-anhydro-4,5,6,8-tetra-O-benzyl-2-deoxy-D-gluco-oct-2-enonic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 13096-62-3
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one

: 108269-37-0
(methoxycarbonylmethylene)tri-n-butylphosphorane

: (E)-3,7-anhydro-4,5,6,8-tetra-O-benzyl-2-deoxy-D-gluco-oct-2-enonic acid methyl ester

: 493018-20-5
(Z)-3,7-anhydro-4,5,6,8-tetra-O-benzyl-2-deoxy-D-gluco-oct-2-enonic acid methyl ester

Guidance literature:: In toluene; at 80 ℃; for 17h;
DOI:10.1016/j.tet.2003.09.081

Reference yield: 80.0%

: 493018-20-5
(Z)-3,7-anhydro-4,5,6,8-tetra-O-benzyl-2-deoxy-D-gluco-oct-2-enonic acid methyl ester

: 124813-78-1
methyl 2-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)acetate

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 23h;
DOI:10.1016/j.tet.2003.09.081