benzyl 1-O-acetyl-6-azido-3,4-di-O-benzyl-3-C,2-O-[(1S)-1-(benzyloxy)ethylene]-6-deoxy-D-glycero-D-gluco-heptopyranuronate

Base Information

Chemical Name:benzyl 1-O-acetyl-6-azido-3,4-di-O-benzyl-3-C,2-O-[(1S)-1-(benzyloxy)ethylene]-6-deoxy-D-glycero-D-gluco-heptopyranuronate
CAS No.:1186486-16-7
Molecular Formula:C₃₉H₃₉N₃O₉
Molecular Weight:693.753
Hs Code.:

Synonyms:benzyl 1-O-acetyl-6-azido-3,4-di-O-benzyl-3-C,2-O-[(1S)-1-(benzyloxy)ethylene]-6-deoxy-D-glycero-D-gluco-heptopyranuronate

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Chemical Property of benzyl 1-O-acetyl-6-azido-3,4-di-O-benzyl-3-C,2-O-[(1S)-1-(benzyloxy)ethylene]-6-deoxy-D-glycero-D-gluco-heptopyranuronate

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Technology Process of benzyl 1-O-acetyl-6-azido-3,4-di-O-benzyl-3-C,2-O-[(1S)-1-(benzyloxy)ethylene]-6-deoxy-D-glycero-D-gluco-heptopyranuronate

There total 1 articles about benzyl 1-O-acetyl-6-azido-3,4-di-O-benzyl-3-C,2-O-[(1S)-1-(benzyloxy)ethylene]-6-deoxy-D-glycero-D-gluco-heptopyranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1186486-13-4
benzyl {methyl 6-azido-3,4-di-O-benzyl-3-C,2-O-[(1S)-1-(benzyloxy)ethylene]-6-deoxy-D-glycero-α-D-gluco-heptopyranosid}uronate

: 108-24-7
acetic anhydride

: 1186486-16-7
benzyl 1-O-acetyl-6-azido-3,4-di-O-benzyl-3-C,2-O-[(1S)-1-(benzyloxy)ethylene]-6-deoxy-D-glycero-D-gluco-heptopyranuronate

Guidance literature:: With sulfuric acid; acetic acid; at -20 - 0 ℃; for 0.25h;
DOI:10.1016/j.bmc.2009.05.057

Reference yield: 65.0%

: 7602-01-9
2-acetamido-6-chloropurine

: 1186486-16-7
benzyl 1-O-acetyl-6-azido-3,4-di-O-benzyl-3-C,2-O-[(1S)-1-(benzyloxy)ethylene]-6-deoxy-D-glycero-D-gluco-heptopyranuronate

: 1186486-19-0
2-(acetylamino)-6-chloro-7-(benzyl {6-azido-3,4-di-O-benzyl-3-C,2-O-[(1S)-1-(benzyloxy)ethylene]-6-deoxy-D-glycero-D-gluco-heptopyranosyl}uronate)purine

Guidance literature:: 2-acetamido-6-chloropurine; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; at 60 ℃; for 0.75h; Inert atmosphere;

benzyl 1-O-acetyl-6-azido-3,4-di-O-benzyl-3-C,2-O-[(1S)-1-(benzyloxy)ethylene]-6-deoxy-D-glycero-D-gluco-heptopyranuronate; With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 65 ℃; for 1.5h; Inert atmosphere;
DOI:10.1016/j.bmc.2009.05.057