2-{4-methoxy-3-[(2-methoxyethoxy)methoxy]phenyl}-2-oxoethyl (3,4,5-trimethoxyphenyl)acetate

Base Information

• Chemical Name: 2-{4-methoxy-3-[(2-methoxyethoxy)methoxy]phenyl}-2-oxoethyl (3,4,5-trimethoxyphenyl)acetate
• CAS No.: 910820-86-9
• Molecular Formula: C₂₄H₃₀O₁₀
• Molecular Weight: 478.496

Synonyms:2-{4-methoxy-3-[(2-methoxyethoxy)methoxy]phenyl}-2-oxoethyl (3,4,5-trimethoxyphenyl)acetate

Chemical Property of 2-{4-methoxy-3-[(2-methoxyethoxy)methoxy]phenyl}-2-oxoethyl (3,4,5-trimethoxyphenyl)acetate

Chemical Property:

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Technology Process of 2-{4-methoxy-3-[(2-methoxyethoxy)methoxy]phenyl}-2-oxoethyl (3,4,5-trimethoxyphenyl)acetate

There total 2 articles about 2-{4-methoxy-3-[(2-methoxyethoxy)methoxy]phenyl}-2-oxoethyl (3,4,5-trimethoxyphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

2-bromo-1-{4-methoxy-3-[(2-methoxyethoxy)methoxy]phenyl}-1-ethanone (910820-85-8) + 3,4,5-trimethoxyphenyl acetic acid (951-82-6) → 2-{4-methoxy-3-[(2-methoxyethoxy)methoxy]phenyl}-2-oxoethyl (3,4,5-trimethoxyphenyl)acetate (910820-86-9)

Guidance literature:

With TEA; In acetonitrile; at 20 ℃; for 15h;

DOI:10.1021/jm060621o

Reference yield:

2-bromo-1-(3-hydroxy-4-methoxyphenyl)-1-ethanone (90971-90-7) → 2-{4-methoxy-3-[(2-methoxyethoxy)methoxy]phenyl}-2-oxoethyl (3,4,5-trimethoxyphenyl)acetate (910820-86-9)

Guidance literature:

Multi-step reaction with 2 steps

1: DIPEA / CH₂Cl₂ / 20 °C

2: 32 percent / TEA / acetonitrile / 15 h / 20 °C

With TEA; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile;

DOI:10.1021/jm060621o

Reference yield: 45.0%

2-{4-methoxy-3-[(2-methoxyethoxy)methoxy]phenyl}-2-oxoethyl (3,4,5-trimethoxyphenyl)acetate (910820-86-9) → 4-{4-methoxy-3-[(2-methoxyethoxy)methoxy]phenyl}-3-(3,4,5-trimethoxyphenyl)-2(5H)-furanone (910820-87-0)

Guidance literature:

With potassium hydroxide; 18-crown-6 ether; In acetonitrile; for 1.5h;

DOI:10.1021/jm060621o

upstream raw materials:

2-bromo-1-{4-methoxy-3-[(2-methoxyethoxy)methoxy]phenyl}-1-ethanone

3,4,5-trimethoxyphenyl acetic acid

2-bromo-1-(3-hydroxy-4-methoxyphenyl)-1-ethanone

Downstream raw materials:

4-{4-methoxy-3-[(2-methoxyethoxy)methoxy]phenyl}-3-(3,4,5-trimethoxyphenyl)-2(5H)-furanone

3-{4-methoxy-3-[(2-methoxyethoxy)methoxy]phenyl}-4-(3,4,5-trimethoxyphenyl)furan

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