4-Benzylamino-9-phenylsulfonyl-1,2,3,4-tetrahydrocarbazol

Base Information

Chemical Name:4-Benzylamino-9-phenylsulfonyl-1,2,3,4-tetrahydrocarbazol
CAS No.:167476-90-6
Molecular Formula:C₂₅H₂₄N₂O₂S
Molecular Weight:416.544
Hs Code.:

Synonyms:4-Benzylamino-9-phenylsulfonyl-1,2,3,4-tetrahydrocarbazol

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Chemical Property of 4-Benzylamino-9-phenylsulfonyl-1,2,3,4-tetrahydrocarbazol

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Technology Process of 4-Benzylamino-9-phenylsulfonyl-1,2,3,4-tetrahydrocarbazol

There total 4 articles about 4-Benzylamino-9-phenylsulfonyl-1,2,3,4-tetrahydrocarbazol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [9-Benzenesulfonyl-1,2,3,9-tetrahydro-carbazol-(4E)-ylidene]-benzyl-amine

: 167476-90-6
4-Benzylamino-9-phenylsulfonyl-1,2,3,4-tetrahydrocarbazol

Guidance literature:: With sodium tetrahydroborate; In methanol; for 4h; Yield given; Ambient temperature;
DOI:10.1002/ardp.19943271003

Reference yield:

: 15128-52-6
1,2,3,9-tetrahydro-4H-carbazol-4-one

: 167476-90-6
4-Benzylamino-9-phenylsulfonyl-1,2,3,4-tetrahydrocarbazol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 80percent NaH / 1.) DMF, 0 deg C, 2.) DMF, r.t., 3 h

2: TiCl₄ / toluene / Ambient temperature

3: NaBH₄ / methanol / 4 h / Ambient temperature

With sodium tetrahydroborate; titanium tetrachloride; sodium hydride; In methanol; toluene;
DOI:10.1002/ardp.19943271003

Reference yield:

: 104876-54-2
9-(phenylsulfonyl)-1,2,3,9-tetrahydro-4H-carbazol-4-one

: 167476-90-6
4-Benzylamino-9-phenylsulfonyl-1,2,3,4-tetrahydrocarbazol

Guidance literature:: Multi-step reaction with 2 steps

1: TiCl₄ / toluene / Ambient temperature

2: NaBH₄ / methanol / 4 h / Ambient temperature

With sodium tetrahydroborate; titanium tetrachloride; In methanol; toluene;
DOI:10.1002/ardp.19943271003