(S)-2-((S)-2-Amino-3-phenyl-propionylamino)-4-methyl-pentanoic acid dimethylamide

Base Information

Chemical Name:(S)-2-((S)-2-Amino-3-phenyl-propionylamino)-4-methyl-pentanoic acid dimethylamide
CAS No.:83892-07-3
Molecular Formula:C₁₇H₂₇N₃O₂
Molecular Weight:305.42
Hs Code.:

Synonyms:(S)-2-((S)-2-Amino-3-phenyl-propionylamino)-4-methyl-pentanoic acid dimethylamide

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Chemical Property of (S)-2-((S)-2-Amino-3-phenyl-propionylamino)-4-methyl-pentanoic acid dimethylamide

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Technology Process of (S)-2-((S)-2-Amino-3-phenyl-propionylamino)-4-methyl-pentanoic acid dimethylamide

There total 8 articles about (S)-2-((S)-2-Amino-3-phenyl-propionylamino)-4-methyl-pentanoic acid dimethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77167-46-5,857478-11-6
L-leucine dimethylamide

: 83892-07-3
(S)-2-((S)-2-Amino-3-phenyl-propionylamino)-4-methyl-pentanoic acid dimethylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 5.99 g / DEPC; Et₃N / dimethylformamide / 12 h / 20 °C

2: TFA / 0.5 h / 20 °C

With triethylamine; diethyl dicarbonate; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/ol990624d

Reference yield:

: 233684-36-1
C₂₂H₃₅N₃O₄

: 83892-07-3
(S)-2-((S)-2-Amino-3-phenyl-propionylamino)-4-methyl-pentanoic acid dimethylamide

Guidance literature:: With trifluoroacetic acid; at 20 ℃; for 0.5h;
DOI:10.1021/ol990624d

Reference yield:

: 13139-15-6,53296-34-7
N-tert-butoxycarbonyl-L-leucine

: 83892-07-3
(S)-2-((S)-2-Amino-3-phenyl-propionylamino)-4-methyl-pentanoic acid dimethylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 4.96 g / DEPC; Et₃N / dimethylformamide / 13 h / 20 °C

2: 5.99 g / DEPC; Et₃N / dimethylformamide / 12 h / 20 °C

3: TFA / 0.5 h / 20 °C

With triethylamine; diethyl dicarbonate; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/ol990624d