C₄₃H₄₈N₄O₉S₂

Base Information

Chemical Name:C₄₃H₄₈N₄O₉S₂
CAS No.:441044-32-2
Molecular Formula:C₄₃H₄₈N₄O₉S₂
Molecular Weight:829.008
Hs Code.:

C<sub>43</sub>H<sub>48</sub>N<sub>4</sub>O<sub>9</sub>S<sub>2</sub>

Synonyms:C₄₃H₄₈N₄O₉S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₃H₄₈N₄O₉S₂

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Technology Process of C₄₃H₄₈N₄O₉S₂

There total 16 articles about C₄₃H₄₈N₄O₉S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 147489-12-1
C₆₄H₆₆N₄O₁₁S₂

: 441044-32-2
C₄₃H₄₈N₄O₉S₂

Guidance literature:: With acetic acid; In water; for 0.333333h;
DOI:10.1021/jo0003910

Reference yield:

: 134056-17-0
(1R,5R,6R,7R)-6-<(benzoyloxy)methyl>-7-<<3-(trifluoromethyl)benzoyl>oxy>-2,8-dioxabicyclo<3.2.1>octane

: 441044-32-2
C₄₃H₄₈N₄O₉S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-methyl-N-trimethylsilyltrifluoroacetamide / acetonitrile / 0.5 h / 20 °C

1.2: 96 percent / SnCl₄ / acetonitrile / 14 h / 20 °C

2.1: 85 percent / Photolysis

3.1: 100 percent / triethylamine / tetrahydrofuran

4.1: NaOH / methanol; H₂O

5.1: PPh₃; diisopropyl azodicarboxylate / tetrahydrofuran

6.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran; methanol / 20 °C

6.2: 93 percent / 1,4-dithioerythritol / methanol; tetrahydrofuran / 0.08 h

7.1: 97 percent / acetic acid / H₂O / 0.33 h

With sodium hydroxide; di-isopropyl azodicarboxylate; N-methyl-N-trimethylsilyl-2,2,2-trifluoroacetamide; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; water; acetonitrile; 1.1: Vorbrueggen reaction / 5.1: Mitsunobu reaction;
DOI:10.1021/jo0003910

Reference yield:

: 134056-18-1
1-<(2R,3R,4R,5R)-3-<<3-(trifluoromethyl)benzoyl>oxy>-4-<(benzoyloxy)methyl>-5-(2-hydroxyethyl)tetrahydrofuran-2-yl>uracil

: 441044-32-2
C₄₃H₄₈N₄O₉S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 85 percent / Photolysis

2.1: 100 percent / triethylamine / tetrahydrofuran

3.1: NaOH / methanol; H₂O

4.1: PPh₃; diisopropyl azodicarboxylate / tetrahydrofuran

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran; methanol / 20 °C

5.2: 93 percent / 1,4-dithioerythritol / methanol; tetrahydrofuran / 0.08 h

6.1: 97 percent / acetic acid / H₂O / 0.33 h

With sodium hydroxide; di-isopropyl azodicarboxylate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; water; 4.1: Mitsunobu reaction;
DOI:10.1021/jo0003910