C₂₉H₃₂I₂N₄O₇

Base Information

Chemical Name:C₂₉H₃₂I₂N₄O₇
CAS No.:1421843-93-7
Molecular Formula:C₂₉H₃₂I₂N₄O₇
Molecular Weight:802.405
Hs Code.:

C<sub>29</sub>H<sub>32</sub>I<sub>2</sub>N<sub>4</sub>O<sub>7</sub>

Synonyms:C₂₉H₃₂I₂N₄O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₃₂I₂N₄O₇

Chemical Property:

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Technology Process of C₂₉H₃₂I₂N₄O₇

There total 7 articles about C₂₉H₃₂I₂N₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77317-55-6
methyl 2-amino-5-iodobenzoate

: 1421843-93-7
C₂₉H₃₂I₂N₄O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

1.2: 51 h / 0 - 20 °C / Inert atmosphere; Reflux

2.1: lithium hydroxide monohydrate / water; methanol / 4 h / 0 °C

3.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 0 - 20 °C

4.1: lithium hydroxide monohydrate / water; methanol / 4 h / 0 °C

With lithium hydroxide monohydrate; chloroformic acid ethyl ester; benzotriazol-1-ol; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1039/c2ob26132d

Reference yield:

: 1408097-83-5
C₃₀H₃₄I₂N₄O₇

: 1421843-93-7
C₂₉H₃₂I₂N₄O₇

Guidance literature:: With lithium hydroxide monohydrate; In methanol; water; at 0 ℃; for 4h;
DOI:10.1039/c2ob26132d

Reference yield:

: 1408097-91-5
C₁₃H₁₅IN₂O₃

: 1421843-93-7
C₂₉H₃₂I₂N₄O₇

Guidance literature:: Multi-step reaction with 2 steps

1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 0 - 20 °C

2: lithium hydroxide monohydrate / water; methanol / 4 h / 0 °C

With lithium hydroxide monohydrate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1039/c2ob26132d