(+/-)-1-tert-butyldiphenylsilyloxy-2-methoxymethylenoxy-3,4-methylenylbutane

Base Information

Chemical Name:(+/-)-1-tert-butyldiphenylsilyloxy-2-methoxymethylenoxy-3,4-methylenylbutane
CAS No.:141619-30-9
Molecular Formula:C₂₃H₃₂O₃Si
Molecular Weight:384.591
Hs Code.:

Synonyms:(+/-)-1-tert-butyldiphenylsilyloxy-2-methoxymethylenoxy-3,4-methylenylbutane

Suppliers and Price of (+/-)-1-tert-butyldiphenylsilyloxy-2-methoxymethylenoxy-3,4-methylenylbutane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of (+/-)-1-tert-butyldiphenylsilyloxy-2-methoxymethylenoxy-3,4-methylenylbutane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of (+/-)-1-tert-butyldiphenylsilyloxy-2-methoxymethylenoxy-3,4-methylenylbutane

There total 2 articles about (+/-)-1-tert-butyldiphenylsilyloxy-2-methoxymethylenoxy-3,4-methylenylbutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 109-87-5
Dimethoxymethane

: 141619-29-6
(+/-)-1-tert-butyldiphenylsilyloxy-3,4-methylenylbutan-2-ol

: 141619-30-9
(+/-)-1-tert-butyldiphenylsilyloxy-2-methoxymethylenoxy-3,4-methylenylbutane

Guidance literature:: With phosphorus pentoxide; In chloroform; for 1h; Ambient temperature;
DOI:10.1080/00397919208021095

Reference yield:

: 177032-63-2
(+/-)-1-(tert-butyldiphenylsilyloxy)-2-hydroxy-3-butene

: 141619-30-9
(+/-)-1-tert-butyldiphenylsilyloxy-2-methoxymethylenoxy-3,4-methylenylbutane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Zn, CuCl / 1.) 80 deg C, 2 h, 2.) glym, 60 deg C, 2 h

2: 50 percent / P₂O₅ / CHCl₃ / 1 h / Ambient temperature

With phosphorus pentoxide; copper(l) chloride; zinc; In chloroform;
DOI:10.1080/00397919208021095