(E)-1-(4-{2-[Bis-(4-fluoro-phenyl)-methoxy]-ethyl}-piperazin-1-yl)-3-(3-methoxy-phenyl)-propenone

Base Information

Chemical Name:(E)-1-(4-{2-[Bis-(4-fluoro-phenyl)-methoxy]-ethyl}-piperazin-1-yl)-3-(3-methoxy-phenyl)-propenone
CAS No.:1026411-48-2
Molecular Formula:C₂₉H₃₀F₂N₂O₃
Molecular Weight:492.566
Hs Code.:

Synonyms:(E)-1-(4-{2-[Bis-(4-fluoro-phenyl)-methoxy]-ethyl}-piperazin-1-yl)-3-(3-methoxy-phenyl)-propenone

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Chemical Property of (E)-1-(4-{2-[Bis-(4-fluoro-phenyl)-methoxy]-ethyl}-piperazin-1-yl)-3-(3-methoxy-phenyl)-propenone

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Technology Process of (E)-1-(4-{2-[Bis-(4-fluoro-phenyl)-methoxy]-ethyl}-piperazin-1-yl)-3-(3-methoxy-phenyl)-propenone

There total 3 articles about (E)-1-(4-{2-[Bis-(4-fluoro-phenyl)-methoxy]-ethyl}-piperazin-1-yl)-3-(3-methoxy-phenyl)-propenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50366-31-9
2-[bis(4-fluorophenyl)methoxy]ethyl chloride

: 1026411-48-2
(E)-1-(4-{2-[Bis-(4-fluoro-phenyl)-methoxy]-ethyl}-piperazin-1-yl)-3-(3-methoxy-phenyl)-propenone

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / K₂CO₃ / toluene / 12 h / Heating

2: dicyclohexylcarbodiimide (DCC) / CH₂Cl₂

With potassium carbonate; dicyclohexyl-carbodiimide; In dichloromethane; toluene; 1: Alkylation / 2: Acylation;
DOI:10.1021/jm990291q

Reference yield:

: 365-24-2
4,4'-difluorobenzhydryl alcohol

: 1026411-48-2
(E)-1-(4-{2-[Bis-(4-fluoro-phenyl)-methoxy]-ethyl}-piperazin-1-yl)-3-(3-methoxy-phenyl)-propenone

Guidance literature:: Multi-step reaction with 3 steps

1: H₂SO₄ / toluene / Heating

2: 69 percent / K₂CO₃ / toluene / 12 h / Heating

3: dicyclohexylcarbodiimide (DCC) / CH₂Cl₂

With sulfuric acid; potassium carbonate; dicyclohexyl-carbodiimide; In dichloromethane; toluene; 1: Condensation / 2: Alkylation / 3: Acylation;
DOI:10.1021/jm990291q