Technology Process of C30H38O6
There total 6 articles about C30H38O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Dess-Martin periodane;
In
dichloromethane; water;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/jo9023039
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triethylamine; pivaloyl chloride / tetrahydrofuran / 2 h / -40 °C / Inert atmosphere
1.2: 18 h / 20 °C / Inert atmosphere
2.1: dimethylaluminum chloride / hexane; dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere
3.1: lithium borohydride / tetrahydrofuran; methanol; diethyl ether / 6 h / 20 °C / Inert atmosphere
4.1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C
5.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere
5.2: 16 h / -78 - 20 °C / Inert atmosphere
6.1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C
With
lithium borohydride; n-butyllithium; dimethylaluminum chloride; pivaloyl chloride; Dess-Martin periodane; triethylamine;
In
tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane;
DOI:10.1002/ejoc.201800262
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere
2.2: 16 h / -78 - 20 °C / Inert atmosphere
3.1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C
With
n-butyllithium; Dess-Martin periodane;
In
tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/ejoc.201800262
