(R)-(3,5,6-trimethylpyrazinyl)methyl 2-acetoxy-3-(3,4-diacetoxyphenyl)propanoate

Base Information

Chemical Name:(R)-(3,5,6-trimethylpyrazinyl)methyl 2-acetoxy-3-(3,4-diacetoxyphenyl)propanoate
CAS No.:1339947-03-3
Molecular Formula:C₂₃H₂₆N₂O₈
Molecular Weight:458.468
Hs Code.:

Synonyms:(R)-(3,5,6-trimethylpyrazinyl)methyl 2-acetoxy-3-(3,4-diacetoxyphenyl)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-(3,5,6-trimethylpyrazinyl)methyl 2-acetoxy-3-(3,4-diacetoxyphenyl)propanoate

Chemical Property:

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Technology Process of (R)-(3,5,6-trimethylpyrazinyl)methyl 2-acetoxy-3-(3,4-diacetoxyphenyl)propanoate

There total 4 articles about (R)-(3,5,6-trimethylpyrazinyl)methyl 2-acetoxy-3-(3,4-diacetoxyphenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.2%

: 1339946-94-9
C₁₇H₂₀N₂O₅

: 108-24-7
acetic anhydride

: 1339947-03-3
(R)-(3,5,6-trimethylpyrazinyl)methyl 2-acetoxy-3-(3,4-diacetoxyphenyl)propanoate

Guidance literature:: dmap; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: 1124-11-4
Tetramethylpyrazine

: 1339947-03-3
(R)-(3,5,6-trimethylpyrazinyl)methyl 2-acetoxy-3-(3,4-diacetoxyphenyl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 70 °C

2: sodium hydrogencarbonate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

3: dmap / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With N-Bromosuccinimide; sodium hydrogencarbonate; dibenzoyl peroxide; dmap; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide;

Reference yield:

: 23028-17-3,42085-50-7,69339-96-4,76822-21-4
danshensu

: 1339947-03-3
(R)-(3,5,6-trimethylpyrazinyl)methyl 2-acetoxy-3-(3,4-diacetoxyphenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: dmap / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With sodium hydrogencarbonate; dmap; In tetrahydrofuran; N,N-dimethyl-formamide;