(2,2-Dichloro-1-{[1-chloro-1-(4-chloro-phenyl)-meth-(Z)-ylidene]-amino}-vinyl)-triphenyl-phosphonium; chloride

Base Information

Chemical Name:(2,2-Dichloro-1-{[1-chloro-1-(4-chloro-phenyl)-meth-(Z)-ylidene]-amino}-vinyl)-triphenyl-phosphonium; chloride
CAS No.:76621-73-3
Molecular Formula:C₂₇H₁₉Cl₄NP*Cl
Molecular Weight:565.693
Hs Code.:

Synonyms:(2,2-Dichloro-1-{[1-chloro-1-(4-chloro-phenyl)-meth-(Z)-ylidene]-amino}-vinyl)-triphenyl-phosphonium; chloride

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Chemical Property of (2,2-Dichloro-1-{[1-chloro-1-(4-chloro-phenyl)-meth-(Z)-ylidene]-amino}-vinyl)-triphenyl-phosphonium; chloride

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Technology Process of (2,2-Dichloro-1-{[1-chloro-1-(4-chloro-phenyl)-meth-(Z)-ylidene]-amino}-vinyl)-triphenyl-phosphonium; chloride

There total 1 articles about (2,2-Dichloro-1-{[1-chloro-1-(4-chloro-phenyl)-meth-(Z)-ylidene]-amino}-vinyl)-triphenyl-phosphonium; chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 55630-07-4
<1-(benzoylamino)-2,2-dichlorovinyl>triphenylphosphonium chloride

: 76621-73-3
(2,2-Dichloro-1-{[1-chloro-1-(4-chloro-phenyl)-meth-(Z)-ylidene]-amino}-vinyl)-triphenyl-phosphonium; chloride

Guidance literature:: With phosphorus pentachloride; In chlorobenzene; at 110 - 120 ℃; for 12h;

Reference yield: 60.0%

: 76621-73-3
(2,2-Dichloro-1-{[1-chloro-1-(4-chloro-phenyl)-meth-(Z)-ylidene]-amino}-vinyl)-triphenyl-phosphonium; chloride

: 152877-47-9,76621-61-9,76621-95-9
<2-(4-chlorophenyl)-5-thioxo-2-thiazolin-4-ylidene>triphenylphosphorane

Guidance literature:: With sodium hydrogensulfide; In N,N-dimethyl-formamide; acetonitrile; at 20 - 25 ℃; for 12h;

Reference yield:

: 76621-73-3
(2,2-Dichloro-1-{[1-chloro-1-(4-chloro-phenyl)-meth-(Z)-ylidene]-amino}-vinyl)-triphenyl-phosphonium; chloride

: 76621-82-4
[2-(4-Chloro-phenyl)-5-methylsulfanyl-thiazol-4-yl]-triphenyl-phosphonium; iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / NaSH / dimethylformamide; acetonitrile / 12 h / 20 - 25 °C

2: 90 percent / methanol

With sodium hydrogensulfide; In methanol; N,N-dimethyl-formamide; acetonitrile;