⁽¹³⁾C₆ phenyl lithium

Base Information

• Chemical Name: ⁽¹³⁾C₆ phenyl lithium
• CAS No.: 112630-78-1
• Molecular Formula: C₆H₅Li
• Molecular Weight: 89.9807

Synonyms:⁽¹³⁾C₆ phenyl lithium

Chemical Property of ⁽¹³⁾C₆ phenyl lithium

Chemical Property:

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Technology Process of ⁽¹³⁾C₆ phenyl lithium

There total 1 articles about ⁽¹³⁾C₆ phenyl lithium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

n-butyllithium (109-72-8,29786-93-4) + bromobenzene-1,2,3,4,5,6-13C6 (112630-77-0,287399-23-9) → (13)C6 phenyl lithium (112630-78-1)

Guidance literature:

In tetrahydrofuran; cyclohexane; at -78 - -50 ℃; for 0.583333h;

Reference yield: 47.0%

(13)C6 phenyl lithium (112630-78-1) + tert-butyl (2R)-2-[methoxy(methyl)carbamoyl]piperidine-1-carboxylate (203056-15-9) → C11(13)C6H23NO3 (907199-99-9)

Guidance literature:

In diethyl ether; hexane; at -23 ℃; for 0.25h;

upstream raw materials:

n-butyllithium

bromobenzene-1,2,3,4,5,6-¹³C₆

Downstream raw materials:

C₁₁⁽¹³⁾C₆H₂₃NO₃

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