15-bromo-9-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-10,12-nonadien-14-ol

Base Information

Chemical Name:15-bromo-9-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-10,12-nonadien-14-ol
CAS No.:103200-80-2
Molecular Formula:C₂₂H₃₅BrO₃
Molecular Weight:427.422
Hs Code.:

Synonyms:15-bromo-9-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-10,12-nonadien-14-ol

Suppliers and Price of 15-bromo-9-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-10,12-nonadien-14-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 15-bromo-9-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-10,12-nonadien-14-ol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 15-bromo-9-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-10,12-nonadien-14-ol

There total 5 articles about 15-bromo-9-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-10,12-nonadien-14-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 103200-76-6
9-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-10,12,14-nonatriene

: 103200-80-2
15-bromo-9-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-10,12-nonadien-14-ol

Guidance literature:: With N-Bromosuccinimide; In 1,4-dioxane; water; at 0 - 5 ℃; for 0.5h;

Reference yield:

: 51077-54-4
9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-9,11-heptadien-13-one

: 103200-80-2
15-bromo-9-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-10,12-nonadien-14-ol

Guidance literature:: Multi-step reaction with 5 steps

1: 63.5 percent / calcium / liquid ammonia; diethyl ether / 3 h / -45 - -40 °C

2: 98 percent / hydrogen / Lindlar's catal. (deact. Pd), quinoline / petroleum ether

3: 97 percent / 5percent sulfuric acid / hexane / 1.75 h / 40 °C

4: 88 percent / pyridine / 120 h / 20 - 25 °C

5: 64 percent / N-bromosuccinimide / dioxane; H₂O / 0.5 h / 0 - 5 °C

With N-Bromosuccinimide; sulfuric acid; hydrogen; calcium; quinoline; Lindlar's catalyst; In 1,4-dioxane; pyridine; diethyl ether; hexane; ammonia; water; Petroleum ether;

Reference yield:

: 103200-77-7
9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-9,11-nonadien-14-yn-13-ol

: 103200-80-2
15-bromo-9-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-10,12-nonadien-14-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / hydrogen / Lindlar's catal. (deact. Pd), quinoline / petroleum ether

2: 97 percent / 5percent sulfuric acid / hexane / 1.75 h / 40 °C

3: 88 percent / pyridine / 120 h / 20 - 25 °C

4: 64 percent / N-bromosuccinimide / dioxane; H₂O / 0.5 h / 0 - 5 °C

With N-Bromosuccinimide; sulfuric acid; hydrogen; quinoline; Lindlar's catalyst; In 1,4-dioxane; pyridine; hexane; water; Petroleum ether;