trifluoro-N-[4-hydroxy-3-(trifluoromethylsulfanyl)phenyl]methanesulfonamide

Base Information

Chemical Name:trifluoro-N-[4-hydroxy-3-(trifluoromethylsulfanyl)phenyl]methanesulfonamide
CAS No.:1309965-43-2
Molecular Formula:C₈H₅F₆NO₃S₂
Molecular Weight:341.255
Hs Code.:

Synonyms:trifluoro-N-[4-hydroxy-3-(trifluoromethylsulfanyl)phenyl]methanesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trifluoro-N-[4-hydroxy-3-(trifluoromethylsulfanyl)phenyl]methanesulfonamide

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Technology Process of trifluoro-N-[4-hydroxy-3-(trifluoromethylsulfanyl)phenyl]methanesulfonamide

There total 2 articles about trifluoro-N-[4-hydroxy-3-(trifluoromethylsulfanyl)phenyl]methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1309965-25-0
trifluoro-N-(4-oxocyclohexa-2,5-dien-1-ylidene)-methanesulfonamide

: tetramethylammonium trifluoromethanethiolate

: 1309965-43-2
trifluoro-N-[4-hydroxy-3-(trifluoromethylsulfanyl)phenyl]methanesulfonamide

Guidance literature:: With acetic acid; In chloroform; at 0 - 20 ℃; for 24h; Inert atmosphere;
DOI:10.1134/S1070428011040075

Reference yield:

: 123-30-8
4-amino-phenol

: 1309965-43-2
trifluoro-N-[4-hydroxy-3-(trifluoromethylsulfanyl)phenyl]methanesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 0 - 20 °C / Inert atmosphere

2: silver(l) oxide / 24 h / Inert atmosphere

3: acetic acid / chloroform / 24 h / 0 - 20 °C / Inert atmosphere

With acetic acid; silver(l) oxide; In diethyl ether; chloroform;
DOI:10.1134/S1070428011040075