4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenylacetate

Base Information

Chemical Name:4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenylacetate
CAS No.:1031401-01-0
Molecular Formula:C₁₄H₁₄F₆O₃
Molecular Weight:344.254
Hs Code.:

Synonyms:4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenylacetate

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Chemical Property of 4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenylacetate

Chemical Property:

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Technology Process of 4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenylacetate

There total 3 articles about 4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1031393-33-5
4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenol

: 108-24-7
acetic anhydride

: 1031401-01-0
4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenylacetate

Guidance literature:: With pyridine; at 20 ℃; for 11h;
DOI:10.1055/s-0036-1588700

Reference yield:

: 1821-39-2
2-propylaniline

: 1031401-01-0
4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenylacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 13 h / 20 - 130 °C / Autoclave

2: sodium nitrite; sulfuric acid / water; 1,4-dioxane / 11.75 h / -10 - 45 °C

3: pyridine / 11 h / 20 °C

With pyridine; sulfuric acid; sodium nitrite; In 1,4-dioxane; water;
DOI:10.1055/s-0036-1588700

Reference yield:

: 2-(4-amino-3-n-propylphenyl)-1,1,1,3,3,3-hexafluoro-propan-2-ol

: 1031401-01-0
4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium nitrite; sulfuric acid / water; 1,4-dioxane / 11.75 h / -10 - 45 °C

2: pyridine / 11 h / 20 °C

With pyridine; sulfuric acid; sodium nitrite; In 1,4-dioxane; water;
DOI:10.1055/s-0036-1588700