N-acetyl-(S)-3-(4’-aminophenyl)-2-methoxypropionic acid

Base Information

Chemical Name:N-acetyl-(S)-3-(4’-aminophenyl)-2-methoxypropionic acid
CAS No.:1240290-49-6
Molecular Formula:C₁₂H₁₅NO₄
Molecular Weight:237.255
Hs Code.:

Synonyms:N-acetyl-(S)-3-(4’-aminophenyl)-2-methoxypropionic acid

Suppliers and Price of N-acetyl-(S)-3-(4’-aminophenyl)-2-methoxypropionic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-acetyl-(S)-3-(4’-aminophenyl)-2-methoxypropionic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-acetyl-(S)-3-(4’-aminophenyl)-2-methoxypropionic acid

There total 8 articles about N-acetyl-(S)-3-(4’-aminophenyl)-2-methoxypropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 921195-94-0
(S)-(-)-3-(4-aminophenyl)-2-methoxypropionic acid

: 108-24-7
acetic anhydride

: 1240290-49-6
N-acetyl-(S)-3-(4’-aminophenyl)-2-methoxypropionic acid

Guidance literature:: In ethyl acetate; at 65 - 70 ℃; for 1.75h; Temperature; Inert atmosphere; Large scale;

Reference yield:

: 103989-25-9
methyl 2-methoxy-3-(4-nitrophenyl)acrylate

: 1240290-49-6
N-acetyl-(S)-3-(4’-aminophenyl)-2-methoxypropionic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: phosphoric acid / water; toluene / 1 h / 25 - 65 °C / pH <= 3 / Large scale

2.1: 5%-palladium/activated carbon; hydrogen / methanol; N,N-dimethyl-formamide / 0 - 80 °C / 2660.18 - 3420.23 Torr / Large scale

3.1: ammonium hydroxide / water / 20 - 30 °C / 760.05 Torr / Large scale

3.2: 0.17 h / 60 - 70 °C / Large scale

4.1: water; acetone / 45 - 55 °C / Inert atmosphere; Large scale

5.1: ammonium hydroxide / water; ethyl acetate / 0.25 h / 20 - 60 °C / Inert atmosphere; Large scale

5.2: 1.5 h / 10 - 60 °C / Inert atmosphere; Large scale

6.1: ethyl acetate / 1.75 h / 65 - 70 °C / Inert atmosphere; Large scale

With ammonium hydroxide; phosphoric acid; 5%-palladium/activated carbon; hydrogen; In methanol; water; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene;

Reference yield:

: 921196-05-6
2-methoxy-3-(4-nitrophenyl)acrylic acid

: 1240290-49-6
N-acetyl-(S)-3-(4’-aminophenyl)-2-methoxypropionic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: 5%-palladium/activated carbon; hydrogen / methanol; N,N-dimethyl-formamide / 0 - 80 °C / 2660.18 - 3420.23 Torr / Large scale

2.1: ammonium hydroxide / water / 20 - 30 °C / 760.05 Torr / Large scale

2.2: 0.17 h / 60 - 70 °C / Large scale

3.1: water; acetone / 45 - 55 °C / Inert atmosphere; Large scale

4.1: ammonium hydroxide / water; ethyl acetate / 0.25 h / 20 - 60 °C / Inert atmosphere; Large scale

4.2: 1.5 h / 10 - 60 °C / Inert atmosphere; Large scale

5.1: ethyl acetate / 1.75 h / 65 - 70 °C / Inert atmosphere; Large scale

With ammonium hydroxide; 5%-palladium/activated carbon; hydrogen; In methanol; water; ethyl acetate; N,N-dimethyl-formamide; acetone;