2,6-dihydroxybenzenecarbothioamide

Base Information

Chemical Name:2,6-dihydroxybenzenecarbothioamide
CAS No.:171017-44-0
Molecular Formula:C₇H₇NO₂S
Molecular Weight:169.204
Hs Code.:

Synonyms:2,6-dihydroxybenzenecarbothioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6-dihydroxybenzenecarbothioamide

Chemical Property:

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Technology Process of 2,6-dihydroxybenzenecarbothioamide

There total 2 articles about 2,6-dihydroxybenzenecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

(EtO)2 P(S)SH: (EtO)2 P(S)SH

: 57764-46-2
2,6-dihydroxybenzonitrile

: 171017-44-0
2,6-dihydroxybenzenecarbothioamide

Guidance literature:: In water;

Reference yield: 43.0%

: 57764-46-2
2,6-dihydroxybenzonitrile

: 171017-44-0
2,6-dihydroxybenzenecarbothioamide

Guidance literature:: With O,O-Diethyl hydrogen phosphorodithioate; In methanol; at 60 ℃; for 36h;

Reference yield:

: 171017-44-0
2,6-dihydroxybenzenecarbothioamide

: (6R,7R)-3-acetyloxymethyl-7-<2-(2,6-dihydroxyphenyl)-4-thiazolyl>acetylamino-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 69 percent / LiBr / tetrahydrofuran

2: 94 percent / 2 N aq. LiOH / tetrahydrofuran; methanol / 0.5 h / 25 °C

3: 66 percent / morpho CDI / tetrahydrofuran; CH₂Cl₂ / 1.) 0 deg C, 24 h, 2.) 25 deg C, 5 h

4: 88 percent / Et₃SiH, trifluoroacetic acid / 1,2-dichloro-ethane / 0 °C

With triethylsilane; lithium hydroxide; morpho CDI; trifluoroacetic acid; lithium bromide; In tetrahydrofuran; methanol; dichloromethane; 1,2-dichloro-ethane;