Technology Process of C27H34N2O*ClH
There total 6 articles about C27H34N2O*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium triacetoxyborate; acetic acid / 1,1-dichloroethane / 14 h / 20 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -20 - -10 °C / Argon gasification
2.2: 2 h / -60 - -20 °C
2.3: 38 h / 20 °C
3.1: hydrogenchloride / methanol
4.1: 10% palladium on activated carbon / ethanol / 17 h / 20 °C / Argon gasification
4.2: 3 h / 60 °C
5.1: hydrogenchloride / methanol
With
hydrogenchloride; n-butyllithium; sodium triacetoxyborate; acetic acid;
10% palladium on activated carbon;
In
tetrahydrofuran; methanol; 1,1-dichloroethane; ethanol; hexane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 18 h / 20 °C
2.1: 10% palladium on activated carbon / ethanol / 17 h / 20 °C / Argon gasification
2.2: 3 h / 60 °C
3.1: hydrogenchloride / methanol
With
hydrogenchloride; sodium hydride;
10% palladium on activated carbon;
In
methanol; DMF (N,N-dimethyl-formamide); ethanol;