(2-{[(tert-butylsulfanyl)methyl]sulfanyl}pyridin-3-yl)(phenyl)methanone

Base Information

Chemical Name:(2-{[(tert-butylsulfanyl)methyl]sulfanyl}pyridin-3-yl)(phenyl)methanone
CAS No.:1436852-55-9
Molecular Formula:C₁₇H₁₉NOS₂
Molecular Weight:317.476
Hs Code.:

Synonyms:(2-{[(tert-butylsulfanyl)methyl]sulfanyl}pyridin-3-yl)(phenyl)methanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-{[(tert-butylsulfanyl)methyl]sulfanyl}pyridin-3-yl)(phenyl)methanone

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Technology Process of (2-{[(tert-butylsulfanyl)methyl]sulfanyl}pyridin-3-yl)(phenyl)methanone

There total 1 articles about (2-{[(tert-butylsulfanyl)methyl]sulfanyl}pyridin-3-yl)(phenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 722541-95-9
C₅H₁₂S₂

: 80100-13-6
(2-bromopyridin-3-yl)(phenyl)methanone

: 1436852-55-9
(2-{[(tert-butylsulfanyl)methyl]sulfanyl}pyridin-3-yl)(phenyl)methanone

Guidance literature:: With sodiumsulfide nonahydrate; In N,N-dimethyl-formamide; at 70 ℃;
DOI:10.1002/hlca.201200123

Reference yield:

: 1436852-55-9
(2-{[(tert-butylsulfanyl)methyl]sulfanyl}pyridin-3-yl)(phenyl)methanone

: C₁₇H₁₉NOS₂

Guidance literature:: With lithium diisopropyl amide; In 1,2-dimethoxyethane; at -78 - 0 ℃; for 0.5h;
DOI:10.1002/hlca.201200123

Reference yield:

: 1436852-55-9
(2-{[(tert-butylsulfanyl)methyl]sulfanyl}pyridin-3-yl)(phenyl)methanone

: 1436852-68-4
2-[(tert-butyl)sulfanyl]-3-phenylthieno[2,3-b]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: lithium diisopropyl amide / 1,2-dimethoxyethane / 0.5 h / -78 - 0 °C

2: thionyl chloride; pyridine / tetrahydrofuran / 1 h / 0 - 20 °C

With pyridine; thionyl chloride; lithium diisopropyl amide; In tetrahydrofuran; 1,2-dimethoxyethane;
DOI:10.1002/hlca.201200123