methyl O-(1,1-dimethylethyl)-N-{[3-[({[2,6-dimethyl-4-(2-propen-1-yl)phenyl]amino}carbonyl)amino]-4'-(methyloxy)-4-biphenylyl]carbonyl}-L-threoninate

Base Information

• Chemical Name: methyl O-(1,1-dimethylethyl)-N-{[3-[({[2,6-dimethyl-4-(2-propen-1-yl)phenyl]amino}carbonyl)amino]-4'-(methyloxy)-4-biphenylyl]carbonyl}-L-threoninate
• CAS No.: 887244-30-6
• Molecular Formula: C₃₅H₄₃N₃O₆
• Molecular Weight: 601.743

Synonyms:methyl O-(1,1-dimethylethyl)-N-{[3-[({[2,6-dimethyl-4-(2-propen-1-yl)phenyl]amino}carbonyl)amino]-4'-(methyloxy)-4-biphenylyl]carbonyl}-L-threoninate

Chemical Property of methyl O-(1,1-dimethylethyl)-N-{[3-[({[2,6-dimethyl-4-(2-propen-1-yl)phenyl]amino}carbonyl)amino]-4'-(methyloxy)-4-biphenylyl]carbonyl}-L-threoninate

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Technology Process of methyl O-(1,1-dimethylethyl)-N-{[3-[({[2,6-dimethyl-4-(2-propen-1-yl)phenyl]amino}carbonyl)amino]-4'-(methyloxy)-4-biphenylyl]carbonyl}-L-threoninate

There total 1 articles about methyl O-(1,1-dimethylethyl)-N-{[3-[({[2,6-dimethyl-4-(2-propen-1-yl)phenyl]amino}carbonyl)amino]-4'-(methyloxy)-4-biphenylyl]carbonyl}-L-threoninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl N-{[3-({[(4-bromo-2,6-dimethylphenyl)amino]carbonyl}amino)-4'-(methyloxy)-4-biphenylyl]carbonyl}-O-(1,1-dimethylethyl)-L-threoninate (887244-29-3) + allyltributylstanane (24850-33-7) → methyl O-(1,1-dimethylethyl)-N-{[3-[({[2,6-dimethyl-4-(2-propen-1-yl)phenyl]amino}carbonyl)amino]-4'-(methyloxy)-4-biphenylyl]carbonyl}-L-threoninate (887244-30-6)

Guidance literature:

bis-triphenylphosphine-palladium(II) chloride; In acetonitrile; at 150 ℃; for 0.0833333h; Irradiation;

Reference yield:

methyl O-(1,1-dimethylethyl)-N-{[3-[({[2,6-dimethyl-4-(2-propen-1-yl)phenyl]amino}carbonyl)amino]-4'-(methyloxy)-4-biphenylyl]carbonyl}-L-threoninate (887244-30-6) → methyl O-(1,1-dimethylethyl)-N-{[3-({[(2,6-dimethyl-4-propylphenyl)amino]carbonyl}amino)-4'-(methyloxy)-4-biphenylyl]carbonyl}-L-threoninate (887244-31-7)

Guidance literature:

With hydrogen; 5% palladium over charcoal; In ethyl acetate; for 1h; under 2585.81 Torr;

upstream raw materials:

methyl N-{[3-({[(4-bromo-2,6-dimethylphenyl)amino]carbonyl}amino)-4'-(methyloxy)-4-biphenylyl]carbonyl}-O-(1,1-dimethylethyl)-L-threoninate

allyltributylstanane

Downstream raw materials:

methyl O-(1,1-dimethylethyl)-N-{[3-({[(2,6-dimethyl-4-propylphenyl)amino]carbonyl}amino)-4'-(methyloxy)-4-biphenylyl]carbonyl}-L-threoninate

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